Solid Oxide Cell Oxygen Electrode Composition for Sr Diffusion Blocking

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Solution Overview

Problem

Solid oxide electrochemical cells face challenges with the formation of high-resistance phases at the interface between the oxygen electrode and the electrolyte, despite the introduction of ceria-based interlayers, due to thermal diffusion of strontium during firing, leading to reduced electrochemical performance.

Innovation Solution

Incorporating a strontium-containing perovskite-type composite oxide with tetravalent elements like titanium or cerium into the oxygen electrode material, which inhibits strontium diffusion and reduces the formation of SrZrO3 at the interface by introducing a rare-earth-doped cerium oxide interlayer between the oxygen electrode and the solid electrolyte.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a ceria-based interlayer is introduced between the oxygen electrode and the electrolyte to prevent SrZrO3 formation, then the interface reaction is suppressed, but SrZrO3 with high resistance is still formed at the interface between the interlayer and the electrolyte due to Sr diffusion during heating

Engineering Contradiction:
Improveinterface stabilityVSAvoidhigh-resistance layer formation
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent introduces a perovskite-type oxide interlayer (e.g., LSMO, LSCO) between the ceria-based interlayer and the YSZ electrolyte. This new interlayer acts as a mediator that blocks Sr diffusion from the oxygen electrode to the electrolyte, preventing SrZrO3 formation at the critical interface while maintaining electrochemical performance.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs a composite structure consisting of multiple interlayers with different functions: a ceria-based interlayer for chemical stability and a perovskite-type oxide interlayer for Sr diffusion blocking. This composite approach combines the advantages of different materials to simultaneously address interface stability and Sr diffusion prevention.

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If the oxygen electrode material is modified with tetravalent elements like Ti or Ce, then Sr diffusion is inhibited and SrZrO3 formation is prevented, but the electrode composition becomes more complex

Engineering Contradiction:
ImproveSr diffusionVSAvoidelectrode material composition
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The patent modifies the oxygen electrode material composition by incorporating tetravalent elements (Ti, Ce) into the perovskite structure. This compositional parameter change alters the diffusion properties of Sr, effectively blocking its migration to the electrolyte interface and preventing high-resistance layer formation.

Inventive Principle:
Principle #35Parameter changes

3Object-affected harmful factors

If Sr diffusion is completely blocked to prevent SrZrO3 formation, then high-resistance phase formation is inhibited, but the electrochemical performance may be affected by excessive Sr retention in the electrode

Engineering Contradiction:
Improvehigh-resistance phase formationVSAvoidelectrochemical performance
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent implements Sr diffusion blocking at the specific location where it is most critical - the interface between the interlayer and the electrolyte. The perovskite-type oxide interlayer provides localized Sr blocking capability at this critical interface, while allowing the bulk electrode to maintain its Sr content for optimal electrochemical performance.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively inhibits the formation of high-resistance phases, enhancing the electrochemical performance and efficiency of both solid oxide fuel cells and electrolysis cells by reducing thermal diffusion of strontium and improving power generation properties.

Implementation Method 1

Sr diffuses through an interlayer from an oxygen electrode, reaches the interface with YSZ, which is a solid electrolyte, and Sr reacts with Zr which has high reactivity with Sr to form SrZrO3

Methodology Applied
Scientific EffectThermal diffusion: Diffusion

Implementation Method 2

when Ti or Ce are doped into an oxygen electrode material, diffusion of Sr is inhibited during heating

Methodology Applied
Scientific EffectThermal diffusion inhibition: Diffusion Barrier

Implementation Method 3

the present inventors have focused on Ti which has higher reactivity with Sr than Zr

Methodology Applied
Scientific EffectChemical reactivity: Chemical Bonding

Implementation Method 4

Sr reacts with Zr which has high reactivity with Sr to form SrZrO3

Methodology Applied
Scientific EffectCompetitive reaction: Chemical Bonding

Implementation Method 5

Solid oxide electrochemical cells include solid oxide electrolysis cells (SOEC) and solid oxide fuel cells (SOFC)

Methodology Applied
Scientific EffectElectrochemical reaction: Fuel Cell

Implementation Method 6

Solid oxide electrochemical cells include solid oxide electrolysis cells (SOEC)

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Data Source

PatentEP4239731A1Solid oxide electrochemical cell and use thereof
Publication Date: 2023.09.06 JAPAN FINE CERAMICS CENTER
  • EP4239731A1 patent drawingFigure 1
  • EP4239731A1 patent drawingFigure 2
  • EP4239731A1 patent drawingFigure 3

AI summary

A solid oxide electrochemical cell includes an oxygen electrode containing a strontium-containing perovskite-type composite oxide represented by Ln1-xSrxCo1-y-zFeyBzO3-δ (Ln is a trivalent lanthanide element, B is a tetravalent element, 0<x<1, 0≤y<1, 0<z<1, and 0<z+y<1, and δ is a value that is determined to satisfy charge neutrality conditions), a solid electrolyte containing zirconium oxide, a hydrogen electrode, and an interlayer containing a rare-earth-doped cerium oxide that is provided between the solid electrolyte and the oxygen electrode.