Solid Source Sublimator Filtration for Stable Vapor Delivery

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Solution Overview

Problem

Existing solid source reactant delivery systems face challenges in efficiently vaporizing and maintaining vapor phase reactants at elevated temperatures to prevent condensation in semiconductor processing, particularly for substances with low vapor pressure, leading to potential clogging and reduced deposition efficiency.

Innovation Solution

A solid source chemical sublimator system comprising a housing with a filter and serpentine flow path, where a filter with controlled porosity restricts the passage of solid reactants, allowing carrier gas to effectively sublimate and saturate with vaporized reactants, and a heating mechanism to maintain the reactants above vaporization temperature, ensuring continuous flow and preventing condensation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a filter with controlled porosity is introduced to restrict solid reactant passage, then clogging is reduced and vaporization efficiency is improved, but device complexity increases

Engineering Contradiction:
Improvevaporization efficiencyVSAvoiddevice complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent applies a filter with controlled porosity to restrict the passage of solid reactants while allowing carrier gas to pass through. This porous filter prevents solid particles from clogging the system while maintaining efficient vaporization of the reactant, directly resolving the contradiction between productivity and device complexity.

Inventive Principle:
Principle #31Porous materials

2Productivity

If heating is intensified to maintain reactants above vaporization temperature, then deposition efficiency is improved, but energy consumption increases

Engineering Contradiction:
Improvedeposition efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent utilizes the phase transition of sublimation for solid reactants with low vapor pressure. By heating the reactant above its sublimation temperature, the solid directly transitions to vapor phase without passing through the liquid phase, enabling efficient deposition while controlling energy consumption through targeted temperature maintenance.

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The patent changes the temperature parameter to maintain reactants above their vaporization temperature. This parameter change enables continuous vaporization and prevents condensation in the processing system, improving deposition efficiency while managing energy requirements through controlled thermal conditions.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If the carrier gas flow rate is increased to prevent condensation, then reactant delivery reliability is improved, but system complexity increases

Engineering Contradiction:
Improvereactant delivery reliabilityVSAvoidsystem complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent uses carrier gas flow through the heated chamber to transport vaporized reactant to the processing zone. The controlled gas flow prevents condensation by maintaining thermal conditions and provides reliable reactant delivery, achieving improved reliability without excessive system complexity through straightforward pneumatic transport.

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system ensures efficient vaporization and delivery of reactants, reducing clogging risks and maintaining reactant vaporization throughout the processing system, thereby enhancing deposition efficiency and extending the time between recharging treatments.

Implementation Method 1

The filter can have a porosity configured to restrict a passage of a solid chemical reactant therethrough

Methodology Applied
Scientific EffectPorosity: Porosity

Implementation Method 2

A solid source chemical sublimator can include a housing configured to hold solid chemical reactant therein

Methodology Applied
Scientific EffectSublimation: Sublimation

Data Source

PatentUS20230383402A1Solid source sublimator
Publication Date: 2023.11.30 ASM IP HLDG BV
  • US20230383402A1 patent drawing
  • US20230383402A1 patent drawing
  • US20230383402A1 patent drawing

AI summary

Herein disclosed are systems and methods related to solid source chemical sublimator vessels and corresponding deposition modules. The solid source chemical sublimator can include a housing configured to hold solid chemical reactant therein. A lid may be disposed on a proximal portion of the housing. The lid can include a fluid inlet and a fluid outlet and define a serpentine flow path within a distal portion of the lid. The lid can be adapted to allow gas flow within the flow path. The solid source chemical sublimator can include a filter that is disposed between the serpentine flow path and the distal portion of the housing. The filter can have a porosity configured to restrict a passage of a solid chemical reactant therethrough.