Solid-State Microwave Generator for Plasma Barrier Deposition

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Solution Overview

Problem

Existing plasma treatment machines for polymer containers, such as PET, face reliability issues, complex assembly processes, and inconsistent plasma activation due to inflexible microwave frequencies produced by magnetrons, leading to poor treatment quality and high discard rates.

Innovation Solution

A plasma-assisted chemical vapor deposition system using a solid-state microwave generator with a frequency variator, coupled with sensors to measure energy intensity and adjust the emission frequency, ensuring stable plasma activation and maintenance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a magnetron is used to generate microwaves for plasma activation, then the machine can operate with conventional proven technology, but the frequency instability and pairing complexity reduce reliability and increase assembly difficulty

Engineering Contradiction:
Improveplasma activation stabilityVSAvoidcavity-magnetron pairing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by using a solid-state microwave generator with adjustable frequency instead of a fixed-frequency magnetron. The control unit dynamically adjusts the microwave frequency to match the resonant frequency of the cavity, ensuring stable plasma activation while eliminating the need for complex manual pairing procedures.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements feedback control by using a sensor to detect plasma characteristics and automatically adjusting the microwave frequency through the control unit. This closed-loop system maintains optimal plasma conditions without requiring manual intervention or complex pre-pairing of components.

Inventive Principle:
Principle #23Feedback

2Reliability

If magnetron frequency is fixed to match cavity resonance, then plasma can be activated, but frequency drift with temperature and voltage changes causes plasma instability

Engineering Contradiction:
Improveplasma maintenance consistencyVSAvoidmicrowave frequency stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent dynamically changes the microwave frequency parameter based on real-time plasma conditions and cavity resonance requirements. The solid-state generator can adjust its output frequency to compensate for temperature and voltage variations, maintaining stable plasma activation without the frequency drift problems of magnetrons.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The control unit continuously monitors plasma characteristics through the sensor and automatically adjusts the microwave frequency to maintain optimal plasma conditions. This feedback mechanism compensates for environmental variations and ensures consistent plasma activation throughout operation.

Inventive Principle:
Principle #23Feedback

3Ease of manufacture

If manual pairing of magnetrons with cavities is performed, then assembly can be completed, but the statistical mismatch rate of 75% increases loss of time and reduces productivity

Engineering Contradiction:
Improvemachine assembly simplicityVSAvoidassembly efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent eliminates the need for manual pairing by using a solid-state generator with adjustable frequency parameters. Any cavity can be matched with any generator by adjusting the frequency, removing the statistical compatibility constraints and simplifying the assembly process.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The solid-state microwave generator is designed to be universally compatible with different cavity types through its adjustable frequency capability. This multi-functionality allows a single generator model to work with various cavity configurations, eliminating the need for specific pairings and streamlining manufacturing.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Device complexity

If bad magnetron-cavity pairing is accepted, then assembly is simplified, but plasma flickers and treatment quality deteriorates, increasing discard rates

Engineering Contradiction:
Improveassembly procedure simplicityVSAvoidplasma treatment quality
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The patent uses dynamic frequency adjustment to ensure optimal plasma conditions regardless of cavity variations. The control unit modifies microwave parameters in real-time to maintain stable plasma and high treatment quality, eliminating the trade-off between assembly simplicity and treatment precision.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The sensor-based feedback system continuously monitors plasma quality and automatically adjusts microwave frequency to maintain optimal treatment conditions. This ensures consistent plasma activation and high treatment quality without requiring complex assembly procedures.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system enhances the reliability and simplicity of machine assembly, improves plasma treatment quality, and reduces discard rates by maintaining consistent plasma intensity and frequency, allowing for efficient deposition of thin barrier layers on container walls.

Implementation Method 1

a microwave generator (15) producing electromagnetic radiation in the microwave frequency range

Methodology Applied
Scientific EffectElectromagnetic radiation: Electromagnetic Induction

Implementation Method 2

activate (and maintain for a predetermined period, generally of the order of a few seconds) in the gas a plasma which dissociates the molecules of the gas

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 3

the resonance frequency of the latter must correspond to an emission frequency peak of the magnetron

Methodology Applied
Scientific EffectElectromagnetic resonance: Resonance

Data Source

PatentEP3292229B1Facility for treating containers by microwave plasma, comprising a solid-state generator and adjustment method
Publication Date: 2020.09.16 SIDEL PARTICIPATIONS SAS
  • EP3292229B1 patent drawingFigure 1~2
  • EP3292229B1 patent drawingFigure 3
  • EP3292229B1 patent drawingFigure 4

AI summary

The invention relates to a facility (1) for plasma-assisted chemical vapour deposition, on an inner wall of a polymer container (2), of a thin barrier layer, and a method for adjusting said facility. The facility (1) comprises: a conductive recess (4); an enclosure (5) mounted in the recess (4); a device (9) for injecting a precursor gas into the enclosure (5); a microwave generator (15); and a device (24) for diffusing microwaves in the enclosure (5), connected to the microwave generator (15), in order to energise and maintain a plasma in the precursor gas; characterised in that the microwave generator (15) is a solid-state generator, provided with a variable frequency drive (22) for the microwave emission frequency; in that it comprises a sensor (13) arranged to measure a physical quantity characterising the energy intensity of the plasma produced in the container (2); and in that it comprises a control unit (14) connected to the sensor (13) and to the microwave generator (15), said control unit (14) being programmed to adjust the microwave emission frequency, via the variable frequency drive (22), in accordance with the value of the physical quantity characterising the energy intensity measured by the sensor (13).