Sorbent Polymer Composite for Flue Gas Mercury Capture

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Solution Overview

Problem

Current methods for removing sulfur oxides, mercury vapor, and fine particulate matters from industrial flue gases face challenges such as corrosion risks, high energy costs, limited adsorbent lifespan, and leaching of halogen sources, which affect the efficiency and durability of pollution control systems.

Innovation Solution

A flue gas treatment device using a sorbent polymer composite substrate with a high surface area support and a hydrophobic polymer, combined with a halogen source having a Langmuir equilibrium constant greater than 10, which is strategically located adjacent to the sorbent material to enhance mercury capture and resist leaching.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If brominated salt is added to pulverized coal for mercury control, then mercury capture efficiency is improved, but corrosion damage from excess bromine and hydrogen bromide increases

Engineering Contradiction:
Improvemercury capture efficiencyVSAvoidcorrosion damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent uses activated carbon as an intermediary substance that facilitates mercury capture through adsorption without introducing corrosive bromine into the flue gas. The activated carbon acts as a mediator between the flue gas and mercury, achieving removal efficiency without the harmful side effects of brominated salt addition.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent extracts the mercury capture function from the combustion process by injecting activated carbon separately into the flue gas stream. This separates the mercury control function from coal combustion, allowing mercury removal without adding brominated compounds to the coal that would cause corrosion.

Inventive Principle:
Principle #2Taking out (Extraction)

2Reliability

If large quantities of powdered activated carbon are injected for high mercury levels, then mercury capture efficiency is improved, but the value of fly ash for concrete sale is compromised

Engineering Contradiction:
Improvemercury capture efficiencyVSAvoidfly ash value
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent changes the operational parameters of carbon injection, specifically controlling the injection rate and location to optimize mercury capture while minimizing carbon carryover into the fly ash. By adjusting these parameters, the system achieves effective mercury removal without compromising fly ash quality for concrete applications.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If fixed bed activated carbon is used for adsorption, then mercury removal is achieved, but adsorbent lifespan is too short for practical applications

Engineering Contradiction:
Improvemercury removal efficiencyVSAvoidadsorbent lifespan
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent transitions from a static fixed bed system to a dynamic fluidized bed system where activated carbon particles are suspended and circulated. This dynamic approach allows continuous contact between the carbon and flue gas, enhancing mercury removal efficiency while extending the effective lifespan of the adsorbent through continuous regeneration and circulation.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements a system where spent activated carbon is continuously regenerated and reused. The carbon is periodically removed, regenerated to restore its adsorption capacity, and returned to the system, thereby extending the overall lifespan of the adsorbent and maintaining continuous mercury removal efficiency.

Inventive Principle:
Principle #34Discarding and recovering

4Reliability

If sorbent polymer composite with halogen source is used, then mercury capture capacity is increased, but halogen source leaching occurs

Engineering Contradiction:
Improvemercury capture capacityVSAvoidhalogen source leaching
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent uses a composite material consisting of activated carbon combined with a sorbent polymer that contains halogen sources. The polymer matrix provides structural support and controlled release of halogen, while the activated carbon provides high surface area for mercury adsorption. This composite structure increases mercury capture capacity while the polymer controls halogen release to minimize leaching.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent utilizes the porous structure of activated carbon within the polymer composite to enhance mercury capture. The porous network provides high surface area for adsorption while the polymer matrix fills the pores to provide structural integrity and control halogen release, preventing leaching while maintaining capture capacity.

Inventive Principle:
Principle #31Porous materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a durable and efficient system for simultaneous removal of SOx, Hg vapor, and PM2.5 with reduced leaching of halogen sources, maintaining effectiveness over a prolonged period and minimizing secondary pollutants, while being cost-effective and environmentally friendly.

Implementation Method 1

a halogen source located adjacent to the SPC substrate where the halogen source has a Langmuir equilibrium constant greater than 10

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a hydrophobic polymer, and a halogen source located adjacent to the SPC substrate

Methodology Applied
Scientific EffectHydrophobic effect: Hydrophobe

Implementation Method 3

simultaneous removal of SOx, Hg vapor, and PM2.5

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP3527279B1A flue gas purification system and process using a sorbent polymer composite material
Publication Date: 2020.11.18 WL GORE & ASSOC INC
  • EP3527279B1 patent drawingFigure 1~2
  • EP3527279B1 patent drawingFigure 3
  • EP3527279B1 patent drawingFigure 3A~4

AI summary

This invention provides a method of removing sulfur oxides, mercury vapor and other contaminants from a flue gas stream and a flue gas treatment device comprising a sorbent polymer composite substrate comprising a high surface area support and a durable halogen source adjacent the sorbent polymer composite substrate. The halogen source comprises a compound with a quaternary ammonium halogen salt that is not washed away.