Sound Sensor Reactor Control for Chlorine Dioxide Decomposition

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Solution Overview

Problem

Chlorine dioxide solutions are unstable and prone to explosive decomposition during production, requiring precise control of chemical reactions to manage heat and reaction rates effectively.

Innovation Solution

A method involving sound sensors to detect reaction events in a reactor, adjusting flow rates based on sound signal comparisons to prevent or mitigate decomposition, using a system that includes a sound sensor adjacent to the reactor, ambient sound detection, and a programmable logic controller to manage feed pumps and valves.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the reaction between metal chlorate/chlorite and strong acid is conducted to generate chlorine dioxide, then chlorine dioxide can be produced at the point of use, but heat is generated and explosive decomposition may occur if not properly controlled

Engineering Contradiction:
Improvechlorine dioxide generationVSAvoidreaction stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The system uses sound sensors to continuously monitor the reactor and provides feedback signals to the control system. When decomposition sounds are detected, the controller adjusts feed rates or activates cooling systems to stabilize the reaction, creating a closed-loop feedback mechanism that prevents explosive decomposition while maintaining productive chlorine dioxide generation

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent replaces traditional mechanical temperature and pressure control systems with an acoustic monitoring system. Sound sensors detect reaction events and decomposition patterns, converting acoustic signals into control actions. This substitution allows for more sensitive and real-time detection of reaction conditions, enabling preventive control before thermal runaway occurs

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If sound sensors are added to detect reaction events and control flow rates, then decomposition can be prevented, but device complexity increases

Engineering Contradiction:
Improvedecomposition preventionVSAvoidsystem complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The sound sensor system serves multiple functions: detecting reaction initiation, monitoring reaction progress, identifying decomposition events, and providing control feedback. By using a single acoustic monitoring approach for multiple detection purposes, the system achieves comprehensive reaction control without proportionally increasing device complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The control system acts as an intermediary between the sound sensors and the chemical reaction process. It receives acoustic signals, processes them to identify reaction events, and translates them into appropriate control actions (adjusting feed rates or activating cooling). This intermediary layer simplifies the overall system architecture by centralizing the control logic

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively controls chemical reactions, preventing unwanted decomposition and ensuring safe, efficient production of chlorine dioxide by identifying and responding to reaction events through sound analysis, thereby stabilizing the reaction process.

Implementation Method 1

detecting a sound in the reactor using a sound sensor that is adjacent to the reactor, wherein the sound sensor converts the sound into a sound signal

Methodology Applied
Scientific EffectSound wave detection and transduction: Sound

Data Source

PatentUS11970393B2Decomposition mediation in chlorine dioxide generation systems through sound detection and control
Publication Date: 2024.04.30 ECOLAB USA INC
  • US11970393B2 patent drawing
  • US11970393B2 patent drawing
  • US11970393B2 patent drawing

AI summary

A method of controlling a chemical reaction is disclosed. The method may include feeding a solution at a first flow rate into a reactor and detecting a sound in the reactor using a sound sensor that is adjacent to the reactor. The sound sensor may convert the sound into a sound signal. After the sound signal is acquired, it is compared to a stored sound signal or a stored sound threshold to detect a reaction event. The method may include adjusting the flow rate of solutions into the reactor in response to the reaction event.