Atomic Absorption Spectrophotometer Frequency-Adaptive Control

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Solution Overview

Problem

The existing atomic absorption spectrophotometers using a double beam optical system face challenges in maintaining optimal lowest detection limit performance due to variations in alternating current power frequency, leading to increased statistical errors and reduced data quality.

Innovation Solution

An atomic absorption spectrophotometer with a light source controller and sampling data extractor that adjust the lighting period and extraction period based on the AC power frequency, ensuring optimal performance independent of the frequency, using a microcomputer chip to set and adjust these parameters for optimal data acquisition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If the lighting period and extraction period are fixed, then the device operation is simple, but the measurement precision deteriorates due to AC power frequency variations

Engineering Contradiction:
Improvedevice operation simplicityVSAvoidlowest detection limit performance
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The patent applies dynamics by making the lighting period and extraction period adjustable parameters that can be optimized based on AC power frequency conditions. The light source controller and sampling data extractor are configured to dynamically adapt their operating parameters to maintain optimal measurement precision under varying frequency conditions, resolving the contradiction between operational simplicity and measurement precision.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent changes the parameters of lighting period and extraction period to optimize measurement precision. By adjusting these temporal parameters in response to AC power frequency variations, the system maintains optimal detection limits without requiring complex operational procedures, thus resolving the contradiction between ease of operation and measurement precision.

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If the lighting period is extended to reduce statistical errors, then the measurement precision improves, but the productivity decreases due to longer measurement cycles

Engineering Contradiction:
Improvestatistical error reductionVSAvoidmeasurement speed
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent employs periodic action by synchronizing the lighting period and extraction period with the sector mirror rotation cycle. This periodic synchronization allows the system to collect sufficient data for high precision measurements while maintaining efficient measurement cycles, thereby resolving the contradiction between reducing statistical errors and maintaining productivity.

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The patent ensures continuity of useful action by coordinating the light source operation and data extraction with the continuous rotation of the sector mirror. This continuous synchronized operation maximizes data collection efficiency during each measurement cycle, improving precision without sacrificing productivity.

Inventive Principle:
Principle #20Continuity of useful action

3Measurement precision

If the light source is continuously ON to maximize data collection, then the measurement precision improves, but the energy consumption increases

Engineering Contradiction:
Improvedata collection qualityVSAvoidlight source energy consumption
Core Design Contradiction:
Measurement precisionVSUse of energy by moving object

Solution Approach 1:

The patent applies periodic action by turning the light source ON and OFF in synchronization with the sector mirror rotation. The light source is activated only during the extraction period when data collection is required, and remains OFF during other periods. This periodic operation maintains high measurement precision while significantly reducing energy consumption compared to continuous operation.

Inventive Principle:
Principle #19Periodic action

4Measurement precision

If the extraction period is extended to improve data quality, then the measurement precision improves, but the time required for each measurement increases

Engineering Contradiction:
Improvedata qualityVSAvoidmeasurement cycle time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent uses periodic action by synchronizing the extraction period with the sector mirror rotation cycle. This synchronization ensures that data extraction occurs at optimal intervals, collecting sufficient high-quality data within each rotation cycle. The periodic timing optimizes the balance between data quality and measurement cycle time, improving precision without excessive time loss.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution ensures consistent optimal lowest detection limit performance by synchronizing the lighting period and data extraction with the sector mirror rotation, reducing statistical errors and maintaining data quality across different AC power frequencies.

Implementation Method 1

a hollow cathode (HC) lamp 11 which is a light source for emitting a light having a bright-line spectrum

Methodology Applied
Scientific EffectBright-line spectrum emission: Luminescence

Implementation Method 2

a deuterium (D2) lamp 12 which is a light source for emitting a light having a continuous spectrum

Methodology Applied
Scientific EffectContinuous spectrum emission: Luminescence

Implementation Method 3

an atomization unit 18 for atomizing a sample

Methodology Applied
Scientific EffectAtomization: Evaporation

Implementation Method 4

a spectroscope 30 for separating the light sent from the sector mirror 21

Methodology Applied
Scientific EffectSpectral separation: Diffraction

Implementation Method 5

a detector 36 for detecting the intensity of the separated light

Methodology Applied
Scientific EffectLight detection: Photoelectric Effect

Implementation Method 6

a half mirror 13 for dividing the light emitted from each lamp into two directions

Methodology Applied
Scientific EffectLight reflection and transmission: Reflection

Implementation Method 7

a sector mirror 21 for sending each light divided by the half mirror 13 to the same optical path

Methodology Applied
Scientific EffectLight reflection: Reflection

Data Source

PatentUS8107072B2Atomic absorption spectrophotometer
Publication Date: 2012.01.31 SHIMADZU CORP
  • US8107072B2 patent drawing
  • US8107072B2 patent drawing
  • US8107072B2 patent drawing

AI summary

The present invention has been accomplished to provide an atomic absorption spectrophotometer capable of obtaining measurement data always in the state where the lowest detection limit performance is optimized, without depending on the frequency of the power supply. In a control program which runs on the microcomputer chip 42 mounted on the atomic absorption spectrophotometer 110, a plurality of lighting periods of the light sources 11 and 12 and extraction periods of the sampling data are memorized, whose lowest detection limit performance are optimized for the frequencies (50 Hz and 60 Hz) of the AC power source for driving the AC motor 22. In using the apparatus, by the control program, the frequency of the power source used in this apparatus is identified, the lighting period and sampling data extraction period corresponding to the identified frequency and the measurement mode that a user of the apparatus has previously set are selected from among a plurality of memorized values, and the appropriate lighting period is set to the hardware (PLD 43). Accordingly, without depending on the frequency, it is possible to obtain measurement data always in the state where the lowest detection limit performance is optimized.