Value-Added Spent FCC Catalyst for Metal-Tolerant RFCC

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Solution Overview

Problem

Current Fluid Catalytic Cracking (FCC) catalysts are not cost-effective for processing heavy metal-laden feeds, leading to catalyst deactivation and the production of undesired products like coke and dry gas, necessitating the development of a more robust and metal-tolerant catalyst for Resid Fluid Catalytic Cracking (RFCC) operations.

Innovation Solution

A value-added spent FCC catalyst composition is created by introducing a rare earth or aluminum component as an activity enhancer, which provides simultaneous metal passivation and catalytic activity enhancement, improving thermal and metal stability, and increasing crystallinity and surface area, allowing for its reuse in RFCC processes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional FCC catalysts are used for processing heavy metal-laden feeds, then catalyst cost is reduced, but catalyst deactivation increases and undesired products are produced

Engineering Contradiction:
Improvecatalyst costVSAvoidcatalyst deactivation
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent modifies the catalyst composition by changing parameters such as adding metal passivators (antimony, arsenic, bismuth compounds) and adjusting the ratio of active components to create a catalyst that resists deactivation by nickel and vanadium while maintaining cost-effectiveness

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite catalyst material combining conventional FCC catalyst components with metal passivators and specific ratios of active components, resulting in a catalyst that simultaneously achieves cost-effectiveness and resistance to metal contamination deactivation

Inventive Principle:
Principle #40Composite materials

2Adaptability or versatility

If high metal tolerance catalysts are developed for RFCC, then processing capability improves, but catalyst complexity increases

Engineering Contradiction:
Improvemetal toleranceVSAvoidcatalyst composition complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent develops a catalyst composition that performs multiple functions simultaneously: it provides catalytic activity for cracking, passivates metals (nickel and vanadium), and maintains thermal stability, thereby achieving metal tolerance without requiring separate additives or complex multi-component systems

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The invention merges the functions of catalytic activity and metal passivation into a single integrated catalyst composition, combining active components with metal passivators in specific ratios to create a unified material that addresses multiple requirements without increasing operational complexity

Inventive Principle:
Principle #5Merging (Combining)

3Ease of manufacture

If spent FCC catalyst is reused for RFCC, then cost is reduced, but thermal stability and metal tolerance are insufficient

Engineering Contradiction:
ImprovecostVSAvoidthermal stability
Core Design Contradiction:
Ease of manufactureVSStability of the object's composition

Solution Approach 1:

The patent applies preliminary treatment to spent FCC catalyst by introducing metal passivators and active components before reuse in RFCC, preparing the catalyst in advance to withstand thermal conditions and metal contamination that would otherwise cause deactivation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention changes the compositional parameters of spent catalyst by adding specific metal passivators (antimony, arsenic, bismuth compounds) and adjusting the ratio of active components, transforming the catalyst properties to achieve thermal stability and metal tolerance suitable for RFCC operation

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The value-added catalyst composition effectively enhances metal tolerance and catalytic activity, improving thermal stability and selectivity, enabling efficient processing of heavy metal-laden feeds and reducing catalyst deactivation rates, thus optimizing RFCC operations and reducing make-up rates.

Implementation Method 1

introducing a rare earth or aluminum component as an activity enhancer, which provides simultaneous metal passivation and catalytic activity enhancement

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

provides simultaneous metal passivation and catalytic activity enhancement

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentUS9266101B2Value added spent fluid catalytic cracking catalyst composition and a process for preparation thereof
Publication Date: 2016.02.23 INDIAN OIL CORP LTD

AI summary

A composition of a value added RFCC catalyst and a process of preparation of a composition for a dual function additive catalyst from a spent catalyst are disclosed. The value added spent FCC catalyst offers improved performance, options such as either employing as an additive for passivation of both vanadium and nickel and enhancing catalytic activity, for initial start-up or make-up for attrition losses. The value addition process does not harm any of physical properties of starting material with respect to ABD, attrition index, surface area and particle size distribution. Value added catalyst can be used in a range from 1-99 wt % in fluid catalytic cracking process in which, feeds may have higher metals and carbon.