Spray Drying Nozzle Tip Cooling via Gas Deflector

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Solution Overview

Problem

Existing spray-drying technologies face challenges in preventing overheating of the spray nozzle tip and denaturation of heat-sensitive substances like proteins during the drying process, leading to reduced potency and potential blockage due to the lack of effective cooling mechanisms for the nozzle tip.

Innovation Solution

A spray-drying apparatus equipped with a drying gas deflector that deflects the flow of drying gas away from the spray nozzle tip, preventing overheating and maintaining the integrity of heat-sensitive substances by minimizing direct exposure to hot gases.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a drying gas conduit is used to provide hot drying gas to dry spray particles, then drying efficiency is improved, but the spray nozzle tip overheats causing denaturation of heat-sensitive substances

Engineering Contradiction:
Improvedrying efficiencyVSAvoidoverheating of spray nozzle tip
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

A cooling gas conduit is introduced as an intermediary element between the drying gas conduit and the spray nozzle tip. The cooling gas flows through this intermediate conduit to protect the spray nozzle tip from direct exposure to hot drying gas, thereby preventing overheating while maintaining drying efficiency in the drying chamber.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The gas flow system is segmented into separate cooling gas and drying gas pathways. The cooling gas conduit and drying gas conduit are distinct, allowing independent control of cooling and drying functions. This segmentation enables the cooling gas to protect the nozzle tip while the drying gas efficiently dries the spray particles in the chamber.

Inventive Principle:
Principle #1Segmentation

2Speed

If high temperature drying gas is used to dry spray particles rapidly, then drying speed is improved, but proteins and heat-sensitive substances undergo denaturation and loss of potency

Engineering Contradiction:
Improvedrying speedVSAvoidpotency of heat-sensitive substances
Core Design Contradiction:
SpeedVSReliability

Solution Approach 1:

The cooling gas acts as a protective intermediary that creates a thermal barrier around the spray nozzle tip and liquid flow path. This allows high-temperature drying gas to be used in the drying chamber for rapid drying, while the cooling gas prevents direct thermal exposure to the heat-sensitive liquid and proteins during atomization.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Different temperature zones are created: a cool zone around the spray nozzle tip and liquid conduit where the cooling gas flows to protect heat-sensitive substances, and a hot zone in the drying chamber where high-temperature drying gas rapidly dries the spray particles. This local differentiation of thermal conditions resolves the contradiction between drying speed and substance integrity.

Inventive Principle:
Principle #3Local quality

3Productivity

If the spray nozzle tip is exposed to hot drying gas, then drying of spray particles is efficient, but sedimentation and blockage of the spray nozzle tip occur

Engineering Contradiction:
Improvedrying efficiencyVSAvoidspray nozzle tip畅通性
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The cooling gas conduit serves as a protective intermediary that prevents direct contact between hot drying gas and the spray nozzle tip. This thermal protection eliminates the cause of sedimentation and blockage, ensuring reliable operation while maintaining drying efficiency through the separate drying gas pathway.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of a drying gas deflector effectively reduces the temperature around the spray nozzle tip, preventing denaturation of proteins and maintaining their potency, while also preventing blockages and ensuring a consistent spray pattern with high yield of dry powder.

Implementation Method 1

a drying gas deflector (40) positioned so as to deflect a flow of drying gas away from the spray nozzle tip

Methodology Applied
Scientific EffectGas flow deflection: Flow Separation

Implementation Method 2

by two-fluid nozzle atomization, wherein spray is created by combination of a liquid flow and a gas flow

Methodology Applied
Scientific EffectTwo-fluid nozzle atomization: Aerosol

Implementation Method 3

drying of the spray in a hot gas (e.g. air) flow provided by a drying gas conduit. The spray particles rapidly dry yielding a powder

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 4

The powder produced is separated from the drying gas by a cyclone unit (30)

Methodology Applied
Scientific EffectCyclone separation: Cyclone Separation

Data Source

PatentEP3221039B1Spray-drying apparatus and method of use
Publication Date: 2020.09.09 OMRIX BIOPHARMACEUTICALS LTD
  • EP3221039B1 patent drawingFigure 1
  • EP3221039B1 patent drawingFigure 2
  • EP3221039B1 patent drawingFigure 3

AI summary

Provided is a spray drying apparatus comprising a spray nozzle comprising a spray nozzle tip at the distal end of the spray nozzle, a liquid conduit for guiding a liquid to be spray-dried out through the spray nozzle tip, an atomizing component for producing a spray of droplets from the liquid exiting the spray nozzle; a drying gas conduit comprising an outlet for directing a drying gas to dry the spray of droplets; and a drying gas deflector positioned so as to deflect a flow of the drying gas away from the spray nozzle tip.