Spray Drying Polymer Dispersant Polysaccharide Mortar Additive

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing dry mortar mixtures face issues with segregation and inhomogeneous distribution of additives due to differences in specific density, grain size, and surface properties, leading to variations in quality and mechanical strength, and the conversion of polysaccharide-based rheology additives into powder form is complex and costly.

Innovation Solution

A method involving the preparation of a powdery composition containing polymeric dispersants with anionic and/or anionogenic groups and polyether side chains, combined with polysaccharides, using an aqueous dispersion with controlled viscosity for spray drying, which results in a rheological additive that prevents segregation and enhances flowability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If polysaccharide-based rheology additives are converted into powder form through traditional methods, then the powder can be used in dry mortar mixes, but the process becomes complex and costly with poor flowability

Engineering Contradiction:
Improvecomplexity of powder production processVSAvoidflowability of powder
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent combines polymeric dispersants and polysaccharides into a single aqueous dispersion before spray drying, creating a unified powdered composition that integrates multiple functions (dispersion and rheology control) into one additive package, simplifying the manufacturing process while maintaining powder flowability

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent changes the physical and chemical parameters of the polysaccharide by combining it with polymeric dispersants in specific weight ratios (1:4 to 1:20), which modifies the dispersion properties and enables successful spray drying without compromising the rheological functionality of the polysaccharide

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If dispersants are added to aqueous slurries to improve workability, then flowability and sprayability improve, but excess dispersant causes water bleeding and segregation

Engineering Contradiction:
Improveworkability of building material mixtureVSAvoidhomogeneity of dry mortar mix
Core Design Contradiction:
Ease of operationVSStability of the object's composition

Solution Approach 1:

The patent creates a homogeneous powdered composition by co-drying polymeric dispersants and polysaccharides together in an aqueous dispersion, ensuring uniform distribution of both components in the final powder, which prevents localized excess concentrations that would cause water bleeding and segregation

Inventive Principle:
Principle #33Homogeneity

Solution Approach 2:

The aqueous dispersion serves as an intermediary medium that allows both polymeric dispersants and polysaccharides to be combined in a controlled manner, enabling precise dosage control and uniform distribution in the final dry mortar mix, preventing the harmful effects of excess dispersant

Inventive Principle:
Principle #24Intermediary (Mediator)

3Strength

If packing density is adjusted to reduce voids in mortar, then mechanical strength improves, but grain sizes must be extremely well matched which is difficult to achieve

Engineering Contradiction:
Improvemechanical strength of mortarVSAvoidflexibility in raw material selection
Core Design Contradiction:
StrengthVSAdaptability or versatility

Solution Approach 1:

The patent extracts the function of void reduction from the physical packing of grains and transfers it to the chemical-rheological domain by using the powdered composition (combining dispersants and polysaccharides) to control water distribution and reduce free water content, allowing normal grain size variations while maintaining strength

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces high-quality, segregation-proof dry mortar mixtures with improved flowability and mechanical strength, reducing the need for grinding steps and optimizing the use of polysaccharides, thus enhancing industrial scalability and cost-effectiveness.

Implementation Method 1

b) spray-drying the aqueous dispersion prepared in process step a)

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP3700967B1Spray drying method
Publication Date: 2024.04.03 BASF SE
  • EP3700967B1 patent drawing
  • EP3700967B1 patent drawing
  • EP3700967B1 patent drawing

AI summary

The invention relates to a method for producing a powdery composition containing at least one polymer dispersant (PD), which comprises structural units having anionic and/or anionogenic groups and structural units having polyether side chains, and at least one polysaccharide (PS). The method comprises the following steps: a) producing an aqueous dispersion, the viscosity of the dispersion being less than 10,000 mPa, containing the at least one polymer dispersant (PD) and the at least one polysaccharide (PS), and b) spray-drying the aqueous dispersion produced in method step a). The invention further relates to the use of the powdery composition according to the invention in inorganic binder compositions, in particular as a rheological additive.