Pneumatic Spray Recirculation for Higher Reaction Yield

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Solution Overview

Problem

Existing spray techniques for generating reaction products face limitations in reaction completion and low product yield due to the limited travel distance of droplets within the spray.

Innovation Solution

A system with a recirculation function is used to collect and re-spray the material, allowing unreacted molecules to react further and incomplete reactions to reach completion, thereby increasing the reaction yield. The system includes a pneumatic sprayer, a collector, and a recirculation loop that allows the unreacted molecules and reaction products to be recycled through the sprayer.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If spray techniques are used to generate reaction products, then reaction rate is accelerated, but reaction completion is limited and product yield is low

Engineering Contradiction:
Improvereaction rateVSAvoidproduct yield
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The system implements continuous recirculation of the liquid spray discharge through the reaction zone. Unreacted molecules are continuously recycled back through the pneumatic sprayer, allowing multiple reaction opportunities and driving the reaction to completion, thereby resolving the contradiction between fast reaction rate and low product yield

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system recovers unreacted molecules from the liquid spray discharge and returns them to the reaction process. By collecting and recirculating the spray material, the system prevents loss of unreacted reagents and maximizes conversion to product, thereby increasing overall product yield while maintaining high reaction rates

Inventive Principle:
Principle #34Discarding and recovering

2Speed

If droplets travel limited distance within the spray, then reaction acceleration occurs, but reaction completion is prevented

Engineering Contradiction:
Improvereaction accelerationVSAvoiddroplet travel distance
Core Design Contradiction:
SpeedVSDuration of action of moving object

Solution Approach 1:

The recirculation system extends the effective duration of droplet reaction by continuously cycling unreacted molecules back through the reaction zone. This maintains the benefits of rapid reaction acceleration while providing multiple opportunities for completion over an extended effective time period

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system employs periodic recirculation cycles where liquid spray discharge is continuously pumped back through the pneumatic sprayer. This periodic action allows droplets to undergo multiple reaction cycles, effectively extending their residence time and enabling complete conversion while preserving the acceleration benefits of each individual spray cycle

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances reaction yield by allowing unreacted molecules to react and incomplete reactions to be driven to completion, while also conserving solvent through condensation and reuse.

Implementation Method 1

a pneumatic sprayer configured to generate a liquid spray discharge from a solvent

Methodology Applied
Scientific EffectPneumatic spray atomization: Spray

Implementation Method 2

The collector may include an electrostatic precipitator

Methodology Applied
Scientific EffectElectrostatic precipitation: Electrostatic Deposition

Implementation Method 3

the solvent may be condensed and reused so that the collected material including unreacted reagents and reaction products is taken up again

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS12325012B2Systems and methods for increasing reaction yield
Publication Date: 2025.06.10 PURDUE RES FOUND
  • US12325012B2 patent drawing
  • US12325012B2 patent drawing
  • US12325012B2 patent drawing

AI summary

The invention generally relates to systems and methods for increasing reaction yield. In certain embodiments, the invention provides systems for increasing a yield of a chemical reaction that include a pneumatic sprayer configured to generate a liquid spray discharge from a solvent. The solvent includes a plurality of molecules, a portion of which react with each other within the liquid spray discharge to form a reaction product. The system also includes a collector positioned to receive the liquid spray discharge including the unreacted molecules and the reaction product. The system also includes a recirculation loop connected from the collector to the pneumatic sprayer in order to allow the unreacted molecules and the reaction product to be recycled through the pneumatic sprayer, thereby allowing a plurality of the unreacted molecules to react with each other as the unreacted molecules cycle again through the system.