Stabilized Complex Hydrides for Hydrogen Storage

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current hydrogen storage technologies, such as metal and complex hydrides, face challenges in achieving high storage capacity, stability, and efficient dehydriding temperatures, particularly for automotive and portable power applications, with existing materials like Al(BH4)3 being unstable and inefficient.

Innovation Solution

Stabilization of aluminum borohydride complexes by adding BH4- groups and metal elements, such as Li, Na, or K, through Lewis base reactions or solvent methods, resulting in more stable and higher capacity hydride compounds like KAl(BH4)4 or LiAl(BH4)4, which can be produced using specific synthesis pathways and stabilization agents.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If complex metal hydrides like Al(BH4)3 are used for hydrogen storage, then high hydrogen storage capacity is achieved, but chemical stability deteriorates

Engineering Contradiction:
Improvehydrogen storage capacityVSAvoidchemical stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent applies composite materials by combining aluminum borohydride with stabilizing agents such as calcium borohydride, lithium borohydride, or amine complexes to form a composite hydrogen storage material. This composite structure maintains the high hydrogen capacity of Al(BH4)3 while the added components provide chemical stability, preventing spontaneous ignition and improving overall material performance for practical hydrogen storage applications.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If conventional hydrogen storage at high pressure (689 bar) is used, then hydrogen storage is achieved, but volumetric efficiency deteriorates

Engineering Contradiction:
Improvehydrogen storageVSAvoidvolumetric efficiency
Core Design Contradiction:
Quantity of substanceVSVolume of moving object

Solution Approach 1:

The patent applies parameter changes by transitioning from gaseous hydrogen storage at high pressure to solid-state complex metal hydride storage. This fundamental parameter change in the physical state of hydrogen storage enables significantly higher volumetric density, as the complex hydrides store hydrogen in a condensed solid form rather than as compressed gas, thereby improving volumetric efficiency for automotive and portable applications.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If complex metal hydrides are used for hydrogen storage, then high storage density is achieved, but dehydriding temperature becomes too high for practical applications

Engineering Contradiction:
Improvestorage densityVSAvoiddehydriding temperature
Core Design Contradiction:
Quantity of substanceVSTemperature

Solution Approach 1:

The patent applies local quality by creating a multi-component system where different components serve specific local functions. The complex metal hydride provides high storage density, while added stabilizing agents and catalysts create localized regions that facilitate hydrogen release at lower temperatures. This spatial and functional differentiation allows the material to maintain high capacity while enabling practical dehydriding temperatures through localized chemical modifications.

Inventive Principle:
Principle #3Local quality

4Stability of the object's composition

If aluminum borohydride is stabilized by adding BH4- groups and metal elements, then chemical stability is improved, but manufacturing complexity increases

Engineering Contradiction:
Improvechemical stabilityVSAvoidmanufacturing complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by pre-synthesizing stable precursor compounds such as calcium borohydride or lithium borohydride that will stabilize the aluminum borohydride during subsequent processing. These preliminary stabilization steps are performed under controlled conditions to ensure chemical stability is established before final material formation, thereby simplifying downstream manufacturing processes and reducing the complexity of handling unstable intermediates.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The stabilized complex hydrides exhibit enhanced chemical stability, higher hydrogen storage capacity, and improved thermodynamic characteristics, enabling efficient hydrogen release at lower temperatures, thus addressing the limitations of existing hydrogen storage materials.

Implementation Method 1

Stabilization of aluminum borohydride complexes by adding BH4- groups and metal elements, such as Li, Na, or K, through Lewis base reactions

Methodology Applied
Scientific EffectLewis base reaction: Chemical Bonding

Implementation Method 2

improved thermodynamic characteristics, enabling efficient hydrogen release at lower temperatures

Methodology Applied
Scientific EffectThermal decomposition: Thermolysis

Data Source

PatentEP2454189B1High capacity stabilized complex hydrides for hydrogen storage
Publication Date: 2020.05.13 SAVANNAH RIVER NUCLEAR SOLUTIONS LLC
  • EP2454189B1 patent drawingFigure 1
  • EP2454189B1 patent drawingFigure 2
  • EP2454189B1 patent drawingFigure 3

AI summary

Complex hydrides based on A1(BH4)3 are stabilized by the presence of one or more additional metal elements or organic adducts to provide high capacity hydrogen storage material.