Self-Reinforced Starch Composite Capsule Material

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Solution Overview

Problem

Gelatin capsules face issues such as reduced solubility, electrostatic charge accumulation, fragility, and non-compatibility with certain religious and faith groups, prompting the need for a biodegradable and vegetarian-friendly alternative with improved mechanical properties.

Innovation Solution

A self-reinforced starch composite is prepared by uniformly mixing oxidized or esterified starch with cross-linked starch or starch nanocrystals, processed through a double screw extruder to form thermoplastic material, which is then extruded into granules or sheets, eliminating the need for additional gel or plasticizers.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If gelatin is used to manufacture capsules, then good biological compatibility and physicochemical properties are achieved, but the capsule shell becomes less soluble and may disintegrate due to crosslinking with aldehyde compounds, reducing sugar compounds, and Vitamin C

Engineering Contradiction:
Improvebiological compatibilityVSAvoidsolubility stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The invention changes the chemical parameters of starch through oxidation, esterification, and crosslinking to achieve the desired gel properties and mechanical strength, replacing gelatin while maintaining capsule functionality and solubility stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite starch materials combining oxidized starch, esterified starch, and crosslinked starch to achieve the required mechanical properties and gel characteristics without using gelatin, thereby avoiding crosslinking-induced solubility issues

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If gelatin is used to manufacture capsules, then good film-forming properties are achieved, but electrostatic charge accumulation occurs in dry conditions, negatively influencing subsequent processing

Engineering Contradiction:
Improvefilm-forming propertiesVSAvoidelectrostatic charge accumulation
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The invention uses starch-based materials that are biodegradable and can be processed without the electrostatic charge accumulation problems of gelatin, providing a sustainable alternative for capsule manufacturing

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Reliability

If gelatin is used to manufacture capsules, then good biological compatibility is achieved, but the capsule becomes fragile and easily broken when stored in low humidity environment for long time

Engineering Contradiction:
Improvebiological compatibilityVSAvoidmechanical strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The invention modifies starch parameters through oxidation, esterification, and crosslinking to achieve optimal gel strength and mechanical properties that maintain capsule integrity during storage in low humidity environments

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention combines multiple modified starch components to create a composite material with enhanced mechanical strength and durability while maintaining biocompatibility, eliminating the fragility issue of gelatin capsules

Inventive Principle:
Principle #40Composite materials

4Adaptability or versatility

If starch is used to replace gelatin, then vegetarian-friendly and biodegradable properties are achieved, but the gel properties of starch itself can hardly meet the requirements of manufacturing process of capsules

Engineering Contradiction:
Improvevegetarian-friendly and biodegradable propertiesVSAvoidprocessing performance
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The invention applies chemical modification parameters (oxidation, esterification, crosslinking) to starch to transform its gel properties and make it suitable for capsule manufacturing processes, achieving both vegetarian-friendly and processable characteristics

Inventive Principle:
Principle #35Parameter changes

5Ease of manufacture

If additional gel or plasticizers are added to improve starch capsule processing performance, then manufacturing processability is improved, but the complexity of the material composition increases and may affect biocompatibility

Engineering Contradiction:
Improveprocessing performanceVSAvoidmaterial composition complexity
Core Design Contradiction:
Ease of manufactureVSDevice complexity

Solution Approach 1:

The invention enables starch to self-reinforce through controlled crosslinking and gel formation, achieving the required mechanical strength and processing performance without needing additional gel agents or plasticizers, thereby maintaining simplicity and biocompatibility

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The self-reinforced starch composite enhances the mechanical and barrier properties of capsule materials, ensuring stability and processability, making it suitable for pharmaceutical and dietary applications while being free from animal-derived components.

Implementation Method 1

heating and kneading the mixture; inputting pure water in an amount of 0.5%-25%, preferably 10%-20%, of the mixture (by weight), thus forming a processable thermoplastic material

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

extruding the thermoplastic material into granules or sheets of self-reinforced material

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentEP2876130B1Preparation process of a self-reinforced starch composite used to produce capsules
Publication Date: 2016.10.05 ZHONGSHAN CAPSULE STARCH MATERIAL TECH
  • EP2876130B1 patent drawingFigure 1
  • EP2876130B1 patent drawing

AI summary

Described is a technical process to prepare a self-reinforced starch composite used to produce capsules. This composite is made by uniformly mixing the matrix phase and the particulate reinforced phase at a proper proportion, the former being one or a combination of the starches selected from the group consisting of oxidized starch, cationic starch and esterified starch ; and the latter, cross-linked starch or starch nanocrystals. This composite is processed into the forms of granules, films, or sheets by extrusion method and these different forms of the composite can be used to replace the gelatin as the raw material of capsules because its barrier property, processability, and mechanical properties are significantly improved.