High-Concentration Starch Milk Viscosity Control

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Solution Overview

Problem

The enzymatic hydrolysis sugar-making process faces challenges in controlling viscosity during the liquefaction stage and achieving high glucose yield due to the limitations of initial starch milk concentration, leading to increased energy consumption and production costs.

Innovation Solution

A method involving a two-step pre-liquefaction process with medium-temperature and high-temperature alpha-amylases, lipase, and neutral protease, followed by flash evaporation and saccharification using a composite enzyme containing pullulanase and glucoamylase, to manage viscosity and enhance glucose yield in starch saccharification products.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the initial concentration of starch milk is increased to improve productivity and reduce energy consumption, then the viscosity of starch during heating gelatinization is sharply increased making liquefaction control difficult

Engineering Contradiction:
Improveinitial starch milk concentrationVSAvoidliquefaction control
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent applies preliminary action by conducting pre-liquefaction treatment before the main heating gelatinization process. Medium-temperature alpha-amylase is added in advance to partially break down starch molecules, reducing the viscosity increase that occurs during subsequent high-temperature gelatinization. This preliminary enzymatic action prepares the starch milk to better withstand high concentrations without becoming uncontrollably viscous.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent utilizes parameter changes by optimizing multiple process parameters simultaneously: controlling pH to 6.0-6.5 for enzyme activity, maintaining temperature at 50-60°C during pre-liquefaction, and adjusting enzyme dosage. These parameter optimizations work together to manage viscosity while maintaining high starch milk concentration, resolving the contradiction between productivity and ease of operation.

Inventive Principle:
Principle #35Parameter changes

2Loss of energy

If the initial concentration of starch milk is increased to reduce energy consumption in evaporation process, then the glucose yield is reduced due to composite reaction generating disaccharide and trisaccharide

Engineering Contradiction:
Improveenergy consumption in evaporationVSAvoidglucose yield
Core Design Contradiction:
Loss of energyVSQuantity of substance

Solution Approach 1:

The patent applies segmentation by dividing the saccharification process into distinct stages with different enzyme systems. First, alpha-amylase performs liquefaction to break down starch into dextrins. Then, glucoamylase and pullulanase are added in a second stage to convert dextrins into glucose while preventing composite reactions. This segmented approach allows high initial starch concentration to be used without reducing glucose yield.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent implements continuity of useful action by maintaining enzymatic hydrolysis throughout the entire process without interruption. The multi-enzyme system ensures continuous conversion of starch to glucose, preventing the accumulation of intermediate products that would otherwise undergo composite reactions. This continuous action maximizes glucose yield even at high starch milk concentrations, eliminating the need for energy-intensive evaporation.

Inventive Principle:
Principle #20Continuity of useful action

3Speed

If spray liquefaction is used to rapidly heat starch milk and limit viscosity increase, then the starch gelatinization phenomenon is still severe and the initial concentration cannot be increased to 35% or more

Engineering Contradiction:
Improveheating speedVSAvoidinitial starch milk concentration
Core Design Contradiction:
SpeedVSProductivity

Solution Approach 1:

The patent applies preliminary action by adding medium-temperature alpha-amylase before the spray liquefaction process. This enzyme begins breaking down starch molecules in advance, creating a more fluid substrate that can be sprayed more effectively. The pre-treated starch milk gelatinizes less severely during rapid heating, allowing higher initial concentrations (40-50%) to be processed through spray liquefaction without clogging or excessive viscosity.

Inventive Principle:
Principle #10Preliminary action

4Temperature

If indirect heating is used to heat starch, then the heating time is too long resulting in excessively high viscosity of the liquefied liquid

Engineering Contradiction:
Improveheating uniformityVSAvoidheating time
Core Design Contradiction:
TemperatureVSDuration of action of moving object

Solution Approach 1:

The patent replaces the mechanical/thermal heating system with an enzymatic system for the pre-liquefaction stage. Instead of relying solely on thermal energy to gelatinize starch, medium-temperature alpha-amylase is used to chemically break down starch molecules at lower temperatures (50-60°C). This substitution dramatically reduces the time required while achieving better viscosity control compared to prolonged indirect heating.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method effectively reduces viscosity, increases the initial starch milk concentration, and improves glucose yield, resulting in reduced energy consumption, increased productivity, and lower production costs while ensuring continuous operation and high filtration rates.

Implementation Method 1

adding medium-temperature alpha-amylase, high-temperature resistant alpha-amylase, lipase and neutral protease into starch milk

Methodology Applied
Scientific EffectEnzymatic hydrolysis: Enzyme

Implementation Method 2

the viscosity of high-concentration starch is sharply increased in the heating gelatinization process

Methodology Applied
Scientific EffectGelatinization:

Implementation Method 3

performing spray liquefaction on the first starch milk, carrying out heat preservation for 3-5 min and then implementing flash evaporation

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 4

adding a composite saccharifying enzyme containing pullulanase and glucoamylase and removing transglucosidase, and carrying out heat preservation and saccharification

Methodology Applied
Scientific EffectEnzymatic hydrolysis: Enzyme

Data Source

PatentUS10808270B2Method for continuously producing starch saccharification products by using high-concentration starch milk
Publication Date: 2020.10.20 COFCO GROUP
  • US10808270B2 patent drawing

AI summary

The present disclosure provides a method for continuously producing starch saccharification products by using high-concentration starch milk.