Starch-Based Superabsorbent Polymer for Saline Soil

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Solution Overview

Problem

Existing superabsorbent polymers experience a significant decrease in water absorbance capacity when exposed to salts, which is problematic in agricultural applications where soil salinity is high, leading to reduced effectiveness in increasing water availability for crops.

Innovation Solution

A process for preparing superabsorbent polymers by graft polymerizing a monomer on a polysaccharide at room temperature, using a catalytic system, and neutralizing the copolymer to produce a starch-based superabsorbent polymer with high water absorbance capacity, avoiding the use of acrylamide and minimizing equipment costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional superabsorbent polymers are used in saline soil conditions, then water absorbance capacity is initially high, but absorbance capacity decreases considerably in the presence of salts

Engineering Contradiction:
Improvewater absorbance capacityVSAvoidsalt interference
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical parameters of the polymer by using starch as a base polymer with grafted acrylic acid and methacrylic acid groups, creating a polymer structure that maintains high water absorbance capacity (100-1500 g/g) even in the presence of salts, unlike conventional polyacrylamide-based SAPs whose absorbance decreases considerably in saline conditions

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite material structure by grafting synthetic acrylic acid and methacrylic acid monomers onto the natural starch polymer backbone, combining the biocompatibility and salt tolerance of starch with the superabsorbent properties of acrylic acid-based polymers, resulting in a material that resists salt interference while maintaining high absorbance

Inventive Principle:
Principle #40Composite materials

2Productivity

If thermal initiation polymerization is used, then polymerization can proceed effectively, but energy consumption increases and reaction conditions become harsh

Engineering Contradiction:
Improvepolymerization efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent replaces thermal initiation (heat-based) with redox initiation using the potassium permanganate/ascorbic acid system, substituting a thermal field with a chemical field that operates at room temperature, thereby eliminating the need for external heating equipment and reducing energy consumption while maintaining effective polymerization

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the initiation mechanism from thermal to redox chemical initiation, allowing polymerization to proceed at room temperature (20-25°C) rather than requiring elevated temperatures, thus reducing energy input while achieving complete polymerization through the selective redox reaction between potassium permanganate and ascorbic acid

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If acrylamide monomer is used, then superabsorbent polymer can be synthesized, but environmental concerns arise and production costs increase

Engineering Contradiction:
Improvesynthesis feasibilityVSAvoidenvironmental impact
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and removes the problematic acrylamide monomer from the synthesis process, replacing it with environmentally benign alternatives (acrylic acid and methacrylic acid) that achieve the same superabsorbent effect without the environmental persistence and toxicity issues associated with acrylamide, thereby eliminating harmful factors while maintaining manufacturing feasibility

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses readily available, inexpensive monomers (acrylic acid and methacrylic acid) that can be easily synthesized or obtained, replacing expensive and environmentally problematic acrylamide, while the resulting polymer maintains its superabsorbent functionality without requiring complex purification or special handling procedures

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting superabsorbent polymer exhibits a high water absorbance capacity of 100 to 1500 g/g, maintaining effectiveness in saline conditions and reducing production costs through environmentally friendly and efficient methods.

Implementation Method 1

graft polymerizing a monomer on a polysaccharide at room temperature

Methodology Applied
Scientific EffectGraft polymerization: Chemical Bonding

Implementation Method 2

using a catalytic system

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

Superabsorbent polymers absorb water or fluids several times their weight

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 4

soluble salts dramatically affect absorption by hydrophilic polyacrylamide gels

Methodology Applied
Scientific EffectHydrophilic interaction: Hydrophile

Implementation Method 5

neutralizing the copolymer to produce a starch-based superabsorbent polymer

Methodology Applied
Scientific EffectNeutralization: Redox Reactions

Data Source

PatentUS20230067242A1Process for preparation of superabsorbent polymer
Publication Date: 2023.03.02 UPL LTD

AI summary

Described herein is a process for preparation of a superabsorbent polymer with high fluid absorptivity. Also described is a composition including the superabsorbent polymer.