Catalytic Steam Reformer Recycle Loop for Turndown Steam

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Solution Overview

Problem

Hydrogen production facilities face challenges in maintaining steam production during turndown conditions, where hydrogen production rates decrease, leading to insufficient export steam due to reduced heat and steam effluent in catalytic steam reformers.

Innovation Solution

A method involving the formation of a reformer feed gas mixture from a steam-containing gas, a sulfur-depleted reformer feedstock, and a separate steam-containing recycle gas mixture, which is introduced into catalytic steam reformer tubes, with external fuel combustion to supply energy, and the subsequent recycling of steam from the boiler effluent to enhance steam production.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If hydrogen production rate is decreased during turndown conditions, then hydrogen production flexibility is improved, but steam production decreases due to reduced heat and steam effluent

Engineering Contradiction:
Improvehydrogen production flexibilityVSAvoidsteam production
Core Design Contradiction:
Adaptability or versatilityVSQuantity of substance

Solution Approach 1:

The invention introduces a feedback mechanism by recycling a portion of the reformer effluent back to the reformer inlet. This recycled stream contains未reacted hydrocarbons and steam, which are reused as feedstock. The feedback loop ensures that even at reduced hydrogen production rates, sufficient steam is maintained in the system through continuous recycling, resolving the contradiction between production flexibility and steam availability

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

Instead of discarding the reformer effluent completely or using it only for its primary purpose (hydrogen production), the invention recovers valuable components from the effluent stream. Specifically, unreacted hydrocarbons and steam are separated and recycled back to the reformer, maximizing resource utilization and maintaining steam production levels regardless of hydrogen production rate

Inventive Principle:
Principle #34Discarding and recovering

2Device complexity

If steam production is coupled directly to hydrogen production rate, then process simplicity is improved, but ability to meet export steam demand during turndown deteriorates

Engineering Contradiction:
Improveprocess complexityVSAvoidsteam demand satisfaction
Core Design Contradiction:
Device complexityVSAdaptability or versatility

Solution Approach 1:

The invention segments the reformer effluent stream into different pathways: one portion continues to the usual downstream processing for hydrogen production, while another portion is diverted and recycled back to the reformer inlet. This segmentation allows independent control of steam production from hydrogen production, enabling the system to meet export steam demands even during turndown conditions without significantly increasing overall process complexity

Inventive Principle:
Principle #1Segmentation

3Adaptability or versatility

If reformer operates at reduced capacity during turndown, then hydrogen production adaptability is improved, but heat transfer efficiency decreases leading to potential overheating risks

Engineering Contradiction:
Improvehydrogen production adaptabilityVSAvoidreformer tube temperature control
Core Design Contradiction:
Adaptability or versatilityVSTemperature

Solution Approach 1:

The recycling of reformer effluent back to the reformer inlet ensures continuous introduction of steam and unreacted hydrocarbons into the reformer tubes. This continuous action maintains adequate heat transfer and prevents localized overheating or coking that could occur during turndown conditions, allowing the reformer to operate adaptively at reduced capacity while maintaining temperature control

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method allows for efficient steam production at various hydrogen production rates, including during turndown conditions, by maintaining heat transfer and reducing energy consumption, thus ensuring steam demand is met while minimizing overheating risks in the reformer tubes.

Implementation Method 1

The reformer feed gas mixture is introduced into a catalytic steam reformer to form a reformed gas mixture

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

In the catalytic steam reformer, hydrocarbon is reformed by steam over a reforming catalyst to form a reformed gas mixture

Methodology Applied
Scientific EffectSteam reforming: Chemical Transport Reactions

Implementation Method 3

Fuel and oxidant, typically air, is introduced through burners generating heat energy that is transferred to the reformer tubes by radiation and convection

Methodology Applied
Scientific EffectCombustion: Combustion

Implementation Method 4

A large portion of the heat contained in this reformed gas mixture is recovered in a heat exchanger, referred to as a waste heat boiler to produce steam

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 5

The separate steam-containing recycle gas mixture may be formed by cooling a first portion of the boiler effluent and compressing the cooled first portion

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentEP1977993B1Catalytic steam reforming with recycle
Publication Date: 2015.11.11 AIR PROD & CHEM INC
  • EP1977993B1 patent drawingFigure 1

AI summary

A method for generating hydrogen in a production facility having a catalytic steam reformer, a boiler downstream of the catalytic steam reformer, optionally having a prereformer, and optionally having a shift reactor, wherein the reformer feed gas mixture is formed using a steam-containing recycle gas mixture which was formed from boiler effluent. The boiler generates steam which may be used to form the reformer feed gas mixture, used elsewhere in the production facility, and/or used for export steam.