Sterically Hindered Amine CO2 Capture with Promoter

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Solution Overview

Problem

Current CO2 capture technologies, such as amine scrubbing, face challenges with high energy requirements, corrosive solutions, and limited efficiency at large scales due to slow reaction rates and high regeneration temperatures, which hinder their economic viability and scalability for large-scale applications like power plants and enhanced oil recovery.

Innovation Solution

The use of sterically hindered amines and tertiary amines with promoter amines, such as piperazine, to enhance CO2 capture and release processes by forming bicarbonate salts, which allows for faster reaction rates and reduced energy consumption through phase changes and precipitation of amine-CO2 reaction products, facilitating more efficient CO2 separation and regeneration.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If conventional aqueous amine scrubbing is used for CO2 capture, then CO2 removal is achieved, but energy consumption is high due to high regeneration temperatures above 100°C

Engineering Contradiction:
Improveenergy consumptionVSAvoidCO2 capture efficiency
Core Design Contradiction:
Use of energy by moving objectVSReliability

Solution Approach 1:

The patent changes the chemical parameters of the amine solution by using sterically hindered amines with specific molecular structures and compositions (20-80 wt% amine, 20-80 wt% water, 1-30 wt% alcohol) that enable effective CO2 capture at lower temperatures, reducing the regeneration temperature requirement while maintaining capture efficiency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite amine solutions combining multiple components (sterically hindered amines, water, and alcohols) that work synergistically to achieve both high CO2 capture efficiency and lower regeneration energy requirements, with the composite formulation optimizing both performance and energy consumption

Inventive Principle:
Principle #40Composite materials

2Productivity

If amine concentration is increased to improve CO2 capture rate, then reaction rate increases, but solution corrosiveness increases

Engineering Contradiction:
ImproveCO2 capture rateVSAvoidsolution corrosiveness
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent optimizes the amine concentration parameter within a specific range (20-80 wt%) and combines it with alcohol additives that modify the solution's chemical properties, reducing corrosiveness while maintaining effective CO2 capture rates through the balanced composition

Inventive Principle:
Principle #35Parameter changes

3Use of energy by stationary object

If conventional amine solutions are used, then CO2 capture is achieved, but heat exchange requirements are high due to large temperature differentials needed for sorption and desorption

Engineering Contradiction:
Improveheat exchange energyVSAvoidCO2 separation efficiency
Core Design Contradiction:
Use of energy by stationary objectVSProductivity

Solution Approach 1:

The patent changes the thermal parameters by using sterically hindered amines that enable effective CO2 sorption at higher temperatures (30-150°C range) compared to conventional amines, reducing the temperature differential between sorption and desorption zones and thereby lowering heat exchange energy requirements while maintaining separation efficiency

Inventive Principle:
Principle #35Parameter changes

4Quantity of substance

If aqueous amine solutions are used for large-scale CO2 capture, then capture capacity is sufficient, but process cost increases due to high energy requirements

Engineering Contradiction:
ImproveCO2 capture capacityVSAvoidprocess cost
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

The patent optimizes multiple parameters simultaneously - amine concentration (20-80 wt%), water content (20-80 wt%), alcohol content (1-30 wt%), and operating temperature (30-150°C) - to achieve a balance between CO2 capture capacity and energy consumption, making large-scale deployment economically viable

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach improves the rate and efficiency of CO2 capture, reduces energy consumption, and enhances the working capacity of CO2 separation systems, making them more viable for large-scale industrial applications by leveraging the promotion of bicarbonate formation and controlled precipitation of amine-CO2 reaction products.

Implementation Method 1

The sorbents mostly used include liquid solvents, as in amine scrubbing processes... Amine scrubbing is based on the chemical reaction of CO2 with amines to generate carbonate/bicarbonate and carbamate salts

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

precipitating at least a portion of the amine-CO2 reaction products to form a precipitate slurry

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Data Source

PatentEP2934724B1Co2 capture from a gas stream by means of a absorption solution comprising amines
Publication Date: 2019.01.02 EXXONMOBIL TECHNOLOGY & ENGINEERING CO
  • EP2934724B1 patent drawingFigure 1~2
  • EP2934724B1 patent drawingFigure 3
  • EP2934724B1 patent drawingFigure 4

AI summary

Promoter amines are used to enhance CO2 uptake by sterically hindered or tertiary amines. The promoter amines can be cyclic amines, including aromatic cyclic amines or bridged cyclic amines. The combination of a promoter amine plus a sterically hindered or tertiary amines allows for improved uptake kinetics while reducing or minimizing the amount of formation of carbamate salts. The promoted sterically hindered or tertiary amines can be used as part of a CO2 capture and release system that involves a phase transition from a solution of amine-CO2 products to a slurry of amine-CO2 precipitate solids.