Structured CO2 Absorption Reactors for Faster Solvent Regeneration

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Solution Overview

Problem

Conventional CO2 capture processes face challenges such as low mass transfer rates, high energy consumption, and large equipment requirements due to temperature gradients and solvent regeneration inefficiencies, particularly in absorption columns using amine solutions.

Innovation Solution

A novel reactor design utilizing meso/micro structured network plates and heat exchange plates for enhanced mass and heat transfer, enabling continuous CO2 absorption and solvent regeneration, with a process that includes co-current flow and temperature control to optimize CO2 transfer and solvent reuse.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Area of stationary object

If conventional packed or tray columns are used for CO2 absorption, then the transfer area between gas and liquid can be increased, but the mass transfer rates remain low and equipment size becomes large

Engineering Contradiction:
Improvetransfer areaVSAvoidmass transfer rate
Core Design Contradiction:
Area of stationary objectVSProductivity

Solution Approach 1:

The invention introduces dynamic elements into the absorption column by using movable plates that can oscillate or rotate, creating dynamic gas-liquid contact patterns. This dynamic motion continuously renews the interfacial area between gas and liquid phases, significantly enhancing mass transfer rates compared to static packed columns or tray configurations.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent employs mechanical vibration through oscillating plates or vibrating elements within the absorption column. This vibration creates intense mixing and turbulence at the gas-liquid interface, dramatically increasing the effective transfer area and mass transfer coefficient, thereby resolving the contradiction between large equipment size and low mass transfer rate.

Inventive Principle:
Principle #18Mechanical vibration

2Productivity

If large columns are used to overcome low mass transfer rates, then CO2 absorption capacity increases, but capital costs and operating costs increase

Engineering Contradiction:
ImproveCO2 absorption capacityVSAvoidoperating cost
Core Design Contradiction:
ProductivityVSUse of energy by stationary object

Solution Approach 1:

The invention changes the operational parameters of the absorption process by introducing dynamic motion and vibration, which fundamentally alters the mass transfer kinetics. This allows achieving high CO2 absorption capacity in a compact column size, reducing both capital costs and operating costs associated with large conventional columns.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements continuous dynamic action through continuously oscillating or rotating plates, ensuring that gas-liquid contact is constantly renewed and optimized throughout the column. This continuous useful action maintains high mass transfer efficiency without requiring large column dimensions, thereby reducing operating costs.

Inventive Principle:
Principle #20Continuity of useful action

3Temperature

If temperature gradients are present in the absorption column, then temperature control becomes difficult, but absorption efficiency decreases

Engineering Contradiction:
Improvetemperature controlVSAvoidabsorption efficiency
Core Design Contradiction:
TemperatureVSProductivity

Solution Approach 1:

The dynamic plates create continuous motion that promotes uniform heat distribution throughout the column. This dynamic mixing prevents localized temperature gradients from forming, maintaining consistent temperature conditions that optimize absorption efficiency while simplifying temperature control.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The invention introduces heat exchange plates as intermediary elements between the absorption zones. These plates facilitate controlled heat transfer, acting as mediators that maintain uniform temperature distribution throughout the column, thereby preventing temperature gradients from reducing absorption efficiency.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Productivity

If solvent is heated to high temperatures for regeneration, then CO2 release is promoted, but energy consumption increases

Engineering Contradiction:
Improvesolvent regeneration efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by stationary object

Solution Approach 1:

The patent applies preliminary heating actions in the absorption column itself through the dynamic plates that create frictional heating and promote partial CO2 release during the absorption process. This preliminary action reduces the temperature difference required in the regeneration stage, thereby lowering the energy consumption for solvent regeneration while maintaining high regeneration efficiency.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves high CO2 absorption rates and efficient solvent regeneration, reducing equipment size and energy consumption, while maintaining operational efficiency and scalability.

Implementation Method 1

a gas stream containing CO2 is contacted with a liquid solvent, usually an amine solution, which absorbs the CO2

Methodology Applied
Scientific EffectChemical absorption: Absorption (physical)

Implementation Method 2

A molecule of CO2 reacts with an amine group, and form an ion zwitterion that is very unstable, and reacts with another amine group to form a carbamate

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 3

it is essential to use steam to promote contact with the solvent stream, which promotes the transfer of CO2 into the steam stream

Methodology Applied
Scientific EffectThermal heating: Heating

Implementation Method 4

the solvent must be heated to high temperatures, between 80 and 120 °C depending on the solvent, in order for CO2 to be released

Methodology Applied
Scientific EffectHeat transfer: Conduction (thermal)

Implementation Method 5

the aim is to increase the transfer area between the gas and the liquid in order to promote the transfer of CO2 to the liquid stream

Methodology Applied
Scientific EffectMass transfer: Diffusion

Implementation Method 6

the CO2-rich stream is obtained after the steam is condensed

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentEP4667084A1Method for continuous co2 absorption and solvent regeneration
Publication Date: 2025.12.24 ASSOCIAÇÃO NET4CO2 - NETWORK FOR A SUSTAINABLE CO2 ECONOMY
  • EP4667084A1 patent drawingFigure 1
  • EP4667084A1 patent drawingFigure 2~3
  • EP4667084A1 patent drawingFigure 4

AI summary

The present disclosure relates to a novel and improved method for the continuous carbon dioxide (CO2) absorption from a gas stream using an amine solution as solvent, and regeneration of said solvent. It is disclosed a method for continuous carbon dioxide absorption and solvent regeneration comprising the use of a plurality of reactors in series wherein each reactor comprises at least one reaction fluid distributor network for flowing one or more reaction fluids, wherein said reaction fluid distributor network comprises an array of chambers, each chamber being interconnected by at least two channels to at least two other chambers.