Sublimation Pressure Control for Stable Precursor Gas Flow

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Solution Overview

Problem

Existing substrate processing systems face challenges in maintaining stable gas pressure during the sublimation of solid precursor materials, leading to inconsistencies in substrate processing, particularly affecting film deposition uniformity.

Innovation Solution

A closed-loop control system is implemented using a pressure sensor to measure the pressure of gaseous precursor downstream of the ampoule, adjusting heater power based on pressure and temperature setpoints to maintain stable gas flow, employing proportional integral control to regulate the sublimation process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If heater power is increased to maintain gas pressure, then gas pressure stability is improved, but energy consumption increases

Engineering Contradiction:
Improvegas pressure stabilityVSAvoidheater energy consumption
Core Design Contradiction:
Stability of the object's compositionVSUse of energy by moving object

Solution Approach 1:

The system employs a pressure sensor to continuously monitor the pressure of gaseous precursor downstream of the ampoule and feeds this information back to the controller. The controller adjusts heater power dynamically based on the measured pressure and a pressure setpoint, increasing power when pressure is low and decreasing power when pressure is high, thereby maintaining stable gas pressure while minimizing energy consumption.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The controller varies the duty cycle of power applied to the heater based on the difference between measured pressure and pressure setpoint. By dynamically changing the power parameter (via duty cycle modulation), the system maintains optimal gas pressure stability while avoiding continuous high energy consumption.

Inventive Principle:
Principle #35Parameter changes

2Stability of the object's composition

If heater power is increased to maintain gas pressure, then gas pressure stability is improved, but film deposition uniformity worsens due to pressure fluctuations

Engineering Contradiction:
Improvegas pressure stabilityVSAvoidfilm deposition uniformity
Core Design Contradiction:
Stability of the object's compositionVSManufacturing precision

Solution Approach 1:

The pressure sensor provides real-time feedback on gas pressure conditions to the controller, which continuously adjusts heater power to maintain pressure at the setpoint. This closed-loop control prevents pressure fluctuations that would otherwise cause inconsistencies in substrate processing and film deposition uniformity.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The system proactively adjusts heater power based on measured pressure deviations from the setpoint, correcting pressure fluctuations before they can significantly impact film deposition. By continuously monitoring and adjusting, the system prevents rather than merely responds to deposition uniformity issues.

Inventive Principle:
Principle #10Preliminary action

3Stability of the object's composition

If pressure sensor is added for closed loop control, then gas pressure stability is improved, but device complexity increases

Engineering Contradiction:
Improvegas pressure stabilityVSAvoidcontrol system complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

A pressure sensor is integrated into the system to provide feedback on the pressure of gaseous precursor downstream of the ampoule. The controller uses this feedback signal to automatically adjust heater power, creating a closed-loop control system that maintains stable gas pressure.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The pressure sensor acts as an intermediary device that bridges the physical gas pressure condition and the electronic control system. By converting pressure information into an electrical signal that the controller can process, the sensor enables automated closed-loop control without requiring complex mechanical or manual intervention systems.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Stabilizes gas pressure input to the mass flow controller, ensuring consistent substrate processing and improved film deposition uniformity by precisely controlling the sublimation of solid precursor materials.

Implementation Method 1

A heater is to heat the ampoule and to sublimate the solid precursor material into a gaseous precursor

Methodology Applied
Scientific EffectSublimation: Sublimation

Data Source

PatentUS12492469B2Sublimation control using downstream pressure sensing
Publication Date: 2025.12.09 LAM RES CORP
  • US12492469B2 patent drawing
  • US12492469B2 patent drawing
  • US12492469B2 patent drawing

AI summary

A system to control gas flow includes an ampoule to store a solid precursor. A heater is to heat the ampoule and to sublimate the solid precursor into a gaseous precursor. A mass flow controller is to regulate a flow of gaseous precursor from the ampoule to a substrate processing chamber. A pressure sensor is to measure a pressure of the gaseous precursor input to the mass flow controller. A controller is to apply power to the electric heater using closed loop control based on the pressure and a pressure setpoint.