Subsurface Alloy Anode for Hydrogen Bromine Flow Battery

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Solution Overview

Problem

H2/Br2 battery systems are susceptible to electrocatalytic surface poisoning due to halide species, which complicates the measurement of bromine species adsorption on platinum-like metals, limiting cell life and efficiency.

Innovation Solution

The anode electrode in the H2/Br2 reduction-oxidation flow battery system is formed with a subsurface alloy of Cu/Pt(111) and/or Au/Pt(111), which reduces bromine adsorption through lower binding energy and maintains facile hydrogen dissociation, thereby resisting poisoning and enhancing battery lifespan.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Power

If a platinum-based catalyst is used in the anode electrode, then hydrogen dissociation is facilitated, but bromine adsorption occurs causing electrode poisoning and reduced cell life

Engineering Contradiction:
Improvehydrogen dissociation capabilityVSAvoidelectrode resistance to poisoning
Core Design Contradiction:
PowerVSReliability

Solution Approach 1:

The patent applies local quality by creating a subsurface alloy structure where Cu or Au atoms are positioned specifically beneath the Pt surface layer. This localized modification changes the electronic structure and binding properties only at the catalyst surface, maintaining hydrogen dissociation activity while reducing bromine adsorption. The subsurface alloying creates a gradient structure with different properties at different depths, optimizing both catalytic activity and poisoning resistance.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent employs composite materials by combining Pt with Cu or Au to form a subsurface alloy composite. This composite structure leverages the complementary properties of the constituent metals: Pt provides excellent hydrogen dissociation catalysis, while Cu or Au in the subsurface position reduces bromine binding energy. The synergistic effect of this composite material resolves the contradiction between maintaining catalytic activity and resisting poisoning.

Inventive Principle:
Principle #40Composite materials

2Power

If the battery system operates with high power capabilities, then energy delivery is improved, but susceptibility to halide poisoning increases, limiting cell life

Engineering Contradiction:
Improvepower capabilitiesVSAvoidcell life
Core Design Contradiction:
PowerVSDuration of action of moving object

Solution Approach 1:

The patent applies parameter changes by modifying the binding energy parameter of the catalyst surface through subsurface alloying. By changing the composition and structure of the catalyst (adding Cu or Au subsurface atoms), the binding energy for bromine is reduced while maintaining hydrogen dissociation capability. This parameter modification allows the system to operate at high power levels without the detrimental effects of strong bromine adsorption, thereby extending cell life.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If conventional electrodes are used, then manufacturing is simpler, but measurement of bromine adsorption is complicated due to poisoning effects

Engineering Contradiction:
Improveelectrode fabricationVSAvoidbromine adsorption measurement
Core Design Contradiction:
Ease of manufactureVSDifficulty of detecting and measuring

Solution Approach 1:

The patent introduces an intermediary approach by using Cu or Au subsurface atoms as mediators between the Pt catalyst surface and bromine species. These intermediary atoms modify the interaction between bromine and the catalyst, reducing adsorption strength. This mediation effect not only protects the electrode but also creates a more measurable system where bromine adsorption can be studied without complete surface blocking, facilitating research and optimization.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of subsurface alloys in the anode electrode reduces bromine adsorption, increasing the battery's lifespan and maintaining high intrinsic reversibility and power capabilities, making it more resistant to poisoning and improving overall performance.

Implementation Method 1

reduces bromine adsorption through lower binding energy

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

maintains facile hydrogen dissociation

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

maintains facile hydrogen dissociation

Methodology Applied
Scientific EffectHydrogen dissociation: Chemical Bonding

Implementation Method 4

an electrolyte containing one or more dissolved electroactive species flows through an electrochemical cell that converts chemical energy to electricity

Methodology Applied
Scientific EffectRedox reactions: Redox Reactions

Data Source

PatentEP2976799B1Redox flow battery system including an anode electrode having a subsurface alloy
Publication Date: 2018.09.12 ROBERT BOSCH GMBH
  • EP2976799B1 patent drawingFigure 1
  • EP2976799B1 patent drawingFigure 2~3
  • EP2976799B1 patent drawingFigure 4

AI summary

A hydrogen/bromine reduction-oxidation flow battery system includes a bromine electrode, a hydrogen electrode, a membrane, a first catalyst, and a second catalyst. The membrane is positioned between the bromine electrode and the hydrogen electrode. The first catalyst is associated with the bromine electrode. The second catalyst is associated with the hydrogen electrode and at least partially formed from a subsurface alloy configured (i) to promote facile dissociation of H2, and (ii) to prevent bromide from adsorbing onto the hydrogen electrode.