Sub-zero Ethanol Extraction for Eco-friendly Absolute Production

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

The cosmetics and perfumery industries face challenges in obtaining eco-friendly absolutes due to the use of toxic and non-renewable solvents like hexane, which are harmful to humans and the environment, and there is a need for a more environmentally friendly process for extracting plant-based fragrances.

Innovation Solution

A process involving ethanolic extraction at temperatures below 0°C, specifically bioethanol extraction at temperatures below −10°C, to extract odorous molecules from plant materials, which replaces traditional solvent-based methods and results in a more sustainable and effective production of absolutes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If traditional organic solvents like hexane are used for extraction, then extraction efficiency is improved, but environmental harm and toxicity increase

Engineering Contradiction:
Improveextraction efficiencyVSAvoidtoxicity and environmental harm
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent changes the temperature parameter by performing extraction at sub-zero temperatures (below 0°C, preferably below -10°C) instead of room temperature. This parameter change enables the use of ethanol as a solvent, which is environmentally friendly and non-toxic, while maintaining effective extraction of odorous molecules from plant material.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces expensive and harmful petrochemical solvents (hexane, heptane, cyclohexane) with bioethanol, which is renewable, non-toxic, and environmentally benign. This substitution eliminates the harmful effects associated with traditional solvents while maintaining extraction effectiveness.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Productivity

If petrochemical solvents are used, then extraction performance is improved, but renewability deteriorates

Engineering Contradiction:
Improveextraction performanceVSAvoidrenewability
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

The patent substitutes non-renewable petrochemical solvents with bioethanol, which is derived from renewable resources. This ensures the extraction process uses renewable materials, aligning with environmental sustainability goals while maintaining extraction performance.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

By changing the temperature parameter to sub-zero conditions, the patent enables the use of bioethanol as an effective solvent, bridging the gap between renewable solvents and extraction efficiency.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If conventional extraction processes are used, then extraction completeness is improved, but extraction time increases

Engineering Contradiction:
Improveextraction completenessVSAvoidextraction time
Core Design Contradiction:
Quantity of substanceVSLoss of time

Solution Approach 1:

The patent changes the temperature parameter to sub-zero conditions, which enhances the extraction rate and completeness. This parameter change allows for faster and more efficient extraction of odorous molecules from plant material compared to conventional room-temperature methods.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process yields absolutes with a comparable or superior olfactive profile to those obtained with hexane, while being free of toxic solvents, and is certified for organic farming standards, offering a faster and more sustainable extraction method that meets stringent environmental and quality certifications.

Implementation Method 1

extracting the plant material in ethanol, preferably bioethanol, at a temperature below 0°C, and more particularly below −10°C

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentUS20240157271A1Process for preparing absolutes
Publication Date: 2024.05.16 INTERNATIONAL FLAVORS & FRAGRANCES INC

AI summary

The present invention relates to a process for the eco-responsible preparation of absolutes that may be used in particular as perfume in the cosmetics and perfumery sectors or as flavour in the food sector. This process is characterized by a step of ethanolic extraction of the plant material at very low temperature.