Sugar Chain-Polypeptide Complex Hydrogel for Broad pH Stability

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Solution Overview

Problem

Current biogels, both of biological and chemical origin, face challenges such as infection risks, immunogenicity, complexity in operation, limited solubility, and applicability issues due to pH-dependent solubility, particularly in the neutral pH range relevant for biological applications like surgery.

Innovation Solution

A sugar chain-polypeptide complex is developed, where a polypeptide with alternating polar and nonpolar amino acid residues is bound to one or more sugar chains, forming a hydrogel with high water-solubility and transparency across a broad pH range, including neutral pH, through self-assembly into a β sheet structure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If biogels of biological origin are used, then high utility value is achieved, but risks of infection and immunogenicity increase

Engineering Contradiction:
Improveutility valueVSAvoidinfection risk
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent employs synthetic peptides that can be manufactured as single-use, sterile products. These synthetic biogels replace biological origin materials that carry infection risks, providing a disposable alternative that eliminates the need for complex sterilization while maintaining high utility value in applications like hemostasis and tissue engineering.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Object-affected harmful factors

If chemical synthesis is used to manufacture biogels, then infection risk is eliminated, but operational complexity increases due to multiple procedures required

Engineering Contradiction:
Improveinfection riskVSAvoidoperational complexity
Core Design Contradiction:
Object-affected harmful factorsVSEase of operation

Solution Approach 1:

The patent segments the gel formation process into distinct functional components within the peptide structure itself. The peptide contains separate domains: one that provides solubility control, another that enables self-assembly, and a third that provides the desired biological function. This segmentation allows the material to automatically perform multiple functions without requiring complex external procedures, reducing operational complexity while maintaining the benefits of chemical synthesis.

Inventive Principle:
Principle #1Segmentation

3Stability of the object's composition

If conventional biogels are used, then gel formation is achieved, but solubility is limited in neutral pH range

Engineering Contradiction:
Improvegel formationVSAvoidsolubility
Core Design Contradiction:
Stability of the object's compositionVSQuantity of substance

Solution Approach 1:

The patent utilizes parameter changes in the peptide structure, specifically incorporating amino acid sequences with alternating polar and nonpolar residues that change their conformational state based on pH. At neutral pH, the peptide maintains high solubility through electrostatic repulsion between charged residues. Upon pH change or ionic strength variation, the peptide undergoes a controlled transition to form gels. This parameter-based control allows tuning of both solubility and gelation properties independently.

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If biogels require buffer exchange or substitution procedures, then gel formation is achieved, but operation becomes complicated and time-consuming

Engineering Contradiction:
Improvegel formationVSAvoidoperation time
Core Design Contradiction:
Stability of the object's compositionVSLoss of time

Solution Approach 1:

The patent designs the peptide to perform self-service functions: the peptide automatically regulates its own solubility and gelation behavior based on environmental conditions without requiring external buffer exchanges or substitutions. The built-in pH-responsive elements and self-assembly domains enable the material to transition from soluble to gel state directly in the application site, eliminating time-consuming laboratory procedures and enabling direct clinical use.

Inventive Principle:
Principle #25Self-service

5Stability of the object's composition

If low solubility biogels are used, then gel structure is formed, but transparency and visibility are reduced

Engineering Contradiction:
Improvegel structureVSAvoidtransparency
Core Design Contradiction:
Stability of the object's compositionVSIllumination intensity

Solution Approach 1:

The patent employs parameter changes to achieve a unique state where the gel maintains high transparency. By carefully controlling the peptide concentration, pH, and ionic strength, the gel forms a homogeneous network structure without micelle formation or phase separation that would cause opacity. The alternating polar-nonpolar amino acid sequence ensures uniform distribution and prevents aggregation, allowing light transmission while maintaining gel integrity and structural stability.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The sugar chain-polypeptide complex forms a uniform and transparent hydrogel, reducing operational complexity, enhancing solubility and applicability, and minimizing antigenicity and toxicity risks, making it suitable for various biological applications including hemostasis and controlled release.

Implementation Method 1

the sugar chain-polypeptide complex may form a hydrogel comprising a β sheet structure by self-assembly in an aqueous solution

Methodology Applied
Scientific EffectSelf-assembly: Self-Assembly

Implementation Method 2

forms a transparent and homogeneous hydrogel in a broad pH range... by self-assembly into a β sheet structure

Methodology Applied
Scientific EffectHydrogen bonding:

Data Source

PatentEP2980098B1(sugar chain)-polypeptide complex
Publication Date: 2018.10.03 GLYTECH LLC
  • EP2980098B1 patent drawingFigure 1~2
  • EP2980098B1 patent drawingFigure 3~4
  • EP2980098B1 patent drawingFigure 5~6

AI summary

The object of the present invention is to provide a sugar chain-polypeptide complex that may form a transparent and homogeneous hydrogel in a broad pH. The present invention provides a sugar chain-polypeptide complex, characterized in that said polypeptide is a polypeptide comprising an amino acid sequence consisting of 8 - 34 amino acid residues in which polar and nonpolar amino acid residues are alternately arranged, and one or more sugar chains are bound to said polypeptide.