Metal Sulfide Roasting via Particle Segmentation and Pelletizing

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Solution Overview

Problem

Current roasting processes face issues with temperature differences within the roaster, leading to incomplete roasting, ferrite formation, and increased sulfide and sulfate sulfur content in calcine particles, which affect downstream leaching steps and metal recovery.

Innovation Solution

Separating concentrate particles into larger pellets before roasting, ensuring at least 80% of the pellets have a diameter of 80% of the average particle size, and pelletizing small calcine particles to achieve homogeneous residence times, reduce sulfation, and minimize sulfide and sulfate sulfur content.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If concentrate particles are roasted in a fluidized bed at high temperatures, then roasting efficiency is improved, but temperature differences between roaster top and bottom increase causing incomplete roasting and ferrite formation

Engineering Contradiction:
Improveroasting efficiencyVSAvoidtemperature difference
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The concentrate particles are separated into different size fractions (fine particles <15 μm and coarse particles ≥15 μm) before roasting. This segmentation allows each fraction to be roasted under optimized conditions, preventing the temperature differences that cause incomplete roasting and ferrite formation while maintaining high roasting efficiency.

Inventive Principle:
Principle #1Segmentation

2Quantity of substance

If small concentrate particles are roasted, then metal yield is improved, but sulfide and sulfate sulfur content in calcine increases affecting downstream leaching

Engineering Contradiction:
Improvemetal yieldVSAvoidsulfide and sulfate sulfur content
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

Fine concentrate particles (<15 μm) are separated and pre-roasted in a separate stream before being combined with coarse particles. This preliminary action ensures complete oxidation of sulfur in fine particles, reducing sulfide and sulfate sulfur content in the final calcine while maintaining high metal yield from the fine particles.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If roasting temperature is increased to improve roasting completeness, then sulfur oxidation is enhanced, but refractory life is reduced and energy consumption increases

Engineering Contradiction:
Improveroasting completenessVSAvoidrefractory life
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

Different temperature regimes are applied to different particle size fractions. Fine particles are roasted at higher temperatures to ensure complete sulfur oxidation, while coarse particles are roasted at moderate temperatures. This local quality approach achieves complete roasting without subjecting the entire system to high temperatures that would reduce refractory life and increase energy consumption.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces temperature differences, enhances roaster capacity, prolongs refractory life, minimizes ferrite formation, and ensures complete oxidation of sulfur and carbon, leading to improved metal recovery and leaching efficiency.

Implementation Method 1

oxidation of small concentrate particles at the top of the roaster occurs

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

thermally treated at temperatures between 500 and 1200 °C in a fluidized bed

Methodology Applied
Scientific EffectFluidization: Fluidisation

Implementation Method 3

gases and at least small particles of the roasted concentrate (calcine) are withdrawn over the top of the roaster and fed into at least one separating device for separating solid particles

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 4

a cooling of the gas-solid-mixture is particularly important

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 5

cyclone(s) connected in parallel or in series

Methodology Applied
Scientific EffectCentrifugal separation: Centrifugal Separation

Implementation Method 6

an electrostatic precipitator (ESP) is foreseen downstream of the separating device

Methodology Applied
Scientific EffectElectrostatic precipitation: Electrostatic Deposition

Data Source

PatentEP3592873B1Process for roasting of metal sulfide concentrates and/or residues
Publication Date: 2024.07.31 METSO METALS OY
  • EP3592873B1 patent drawingFigure 1
  • EP3592873B1 patent drawingFigure 2
  • EP3592873B1 patent drawingFigure 3

AI summary

The invention describes a process for roasting of metal concentrate. Concentrate particles are fed into a roaster where they are thermally treated at a temperature in the range of 500 and 1200°C in a fluidized bed to form a calcine. At least parts of the calcine are withdrawn from the roaster together with a gas stream as a solid fraction. Concentrate particles with a diameter at least 50% smaller than the average diameter of the concentrate particles are separated as small particles and/or that particles from the gas-solid-fraction are separated in at least one step as small calcine particles and/or that particles are gained in another hydrometallurgical step as other particles. The small particles and/or at least part of the small calcine particles and/or at least parts of the other particles are pelletized, whereby at least 80 % of the pellets feature a diameter of at least 80% of the concentrate particles average diameter. The pellets are fed into the roaster.