Sunflower Oleosome Concentrate With Two-Stage pH Separation

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Solution Overview

Problem

Existing processes for isolating sunflower oleosome concentrates result in products with lower robustness, nutritional profile, and sensorial characteristics, particularly when maximizing yield.

Innovation Solution

A process involving grinding sunflower seeds in an alkaline aqueous solution to create a slurry with pH 7.2 to 9.0, isolating a sunflower oleosome fraction, and washing at pH 6.6 to 7.0 to produce a concentrate with 13.0 to 17.0% protein and 83.0 to 87.0% lipid content, primarily as oleosomes, without using organic solvents.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If existing processes maximize oleosome concentrate yield, then productivity is improved, but robustness, nutritional profile and sensorial characteristics deteriorate

Engineering Contradiction:
Improveoleosome concentrate yieldVSAvoidoleosome concentrate robustness
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies parameter changes by controlling pH at two distinct stages: maintaining pH 7.2-9.0 during grinding and isolation to maximize yield, then adjusting to pH 6.6-7.0 during washing to improve robustness and nutritional profile. This sequential parameter adjustment resolves the contradiction between productivity and product quality.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If existing processes maximize oleosome concentrate yield, then productivity is improved, but nutritional profile deteriorates

Engineering Contradiction:
Improveoleosome concentrate yieldVSAvoidprotein content
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The patent uses parameter changes through pH control to simultaneously achieve high yield and high protein content. The washing step at pH 6.6-7.0 specifically enhances protein retention in the oleosome concentrate while maintaining productivity, resolving the contradiction between quantity of substance and productivity.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If existing processes maximize oleosome concentrate yield, then productivity is improved, but sensorial characteristics deteriorate

Engineering Contradiction:
Improveoleosome concentrate yieldVSAvoidsensorial quality
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent applies parameter changes by implementing a two-stage pH control system. The final washing at pH 6.6-7.0 optimizes sensorial characteristics including creaminess and mouthfeel, while the overall process maintains high productivity through efficient isolation at pH 7.2-9.0.

Inventive Principle:
Principle #35Parameter changes

4Productivity

If washing is performed at high pH to maintain yield, then productivity is improved, but stability deteriorates

Engineering Contradiction:
Improveoleosome concentrate yieldVSAvoidoleosome concentrate stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The patent resolves this contradiction by changing the pH parameter during washing to 6.6-7.0, which is lower than the isolation pH but still maintains acceptable yield while significantly improving stability. This parameter optimization ensures both productivity and compositional stability.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process yields a stable, high-protein sunflower oleosome concentrate with minimal free oil and enhanced nutritional and sensory qualities, allowing for improved product stability and functionality in food, feed, and other applications.

Implementation Method 1

Grinding sunflower seeds in the presence of an aqueous solution and obtaining a sunflower seed slurry having a pH in a range of from more than 7.2 to 9.0

Methodology Applied
Scientific EffectpH adjustment:

Implementation Method 2

Said suspension is centrifuged to separate the oleosomes from the remaining seed content and obtain an oleosome concentrate

Methodology Applied
Scientific EffectCentrifugal separation: Centrifugal Separation

Implementation Method 3

Washing the sunflower oleosome fraction at a pH in a range of from 6.6 to 7.0 and isolating the sunflower oleosome concentrate

Methodology Applied
Scientific EffectpH adjustment:

Data Source

PatentEP4472430B1Sunflower oleosome concentrate and process for preparing it
Publication Date: 2025.11.26 CARGILL INC

AI summary

Invention describes a process for preparing a sunflower oleosome concentrate; comprising steps of a) grinding sunflower seeds in the presence of aqueous solution and obtaining a sunflower seed slurry having a pH from more than 7.2 to 9.0, b) isolating a sunflower oleosome fraction, and c) washing it in an aqueous salt solution at a pH in a range of from 6.6 to 7.0. Invention further relates to a sunflower oleosome concentrate with a protein content of from more than 13 to 17 wt.%. Invention relates to a process for preparing food and feed products, nutritional compositions and others.