Superabsorbent Polymer Gel for Cellulose-Free Diaper Leakage

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Solution Overview

Problem

Current superabsorbents are inadequately suited for the new generation of cellulose-free diaper constructions, which require enhanced hydrogel properties to prevent urine leakage during micturition and optimize liquid distribution.

Innovation Solution

Development of particulate absorbent polymer materials with specific properties, including high centrifuge retention capacity and absorption under pressure, achieved through radical polymerization and surface post-crosslinking, to effectively immobilize and distribute absorbed liquids.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Volume of moving object

If superabsorbent particles are immobilized on substrate surface using thermoplastic fibers, then the absorbent core can be made thinner with reduced cellulose fiber content, but the ability to prevent urine leakage during micturition deteriorates

Engineering Contradiction:
Improveabsorbent core thicknessVSAvoidleakage prevention capability
Core Design Contradiction:
Volume of moving objectVSReliability

Solution Approach 1:

The patent applies parameter changes by modifying the surface properties of superabsorbent particles through post-crosslinking treatment. This changes the gel structure and surface characteristics of the particles, enabling them to effectively prevent urine leakage during micturition even in thin, cellulose-free absorbent cores. The crosslinking density and gel composition are adjusted to optimize both leakage prevention and absorption performance.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure by combining superabsorbent particles with specific gel-forming components and thermoplastic fibers. The superabsorbent particles are treated to form a composite gel matrix that works synergistically with the thermoplastic fiber network to provide both structural integrity and leakage prevention, replacing the traditional cellulose fiber function.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If cellulose fiber content is reduced in absorbent cores, then wearing comfort and packaging costs are improved, but the temporary liquid storage and transfer function deteriorates

Engineering Contradiction:
Improvecellulose fiber contentVSAvoidliquid storage and transfer function
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent changes the parameters of superabsorbent particles through controlled crosslinking and gel formation. The gel structure is engineered to provide temporary liquid storage capacity, replacing the cellulose fiber function. The gel's swelling properties and network structure are optimized to hold liquid temporarily before transfer to the reservoir layer.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces a gel-forming component as an intermediary between the superabsorbent particles and the liquid. This gel acts as a temporary storage medium, facilitating liquid retention and controlled release, thereby compensating for the removed cellulose fiber function in liquid storage and transfer.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Quantity of substance

If superabsorbent content is increased to compensate for lost cellulose fiber function, then absorption capacity is maintained, but the ability to distribute liquid throughout the gel layer deteriorates

Engineering Contradiction:
Improvesuperabsorbent contentVSAvoidliquid distribution capability
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent utilizes porous gel structures formed by the crosslinked superabsorbent particles. The gel network creates interconnected pores that facilitate liquid distribution throughout the absorbent core. This porous structure allows liquid to penetrate and distribute evenly across the gel layer, preventing pooling and ensuring uniform absorption even with high superabsorbent content.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent adjusts the crosslinking parameters and gel composition to optimize liquid distribution. By controlling the gel's mesh size, swelling ratio, and surface hydrophilicity, the liquid can be effectively distributed throughout the gel layer while maintaining high absorption capacity with increased superabsorbent content.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new absorbent polymer materials provide improved leakage prevention and optimal liquid distribution within the diaper, enhancing the performance of cellulose-free absorbent cores.

Implementation Method 1

Superabsorbents are water-insoluble, cross-linked polymers that are capable of absorbing large amounts of aqueous liquids, in particular body fluids, preferably urine or blood, while swelling and forming hydrogels, and retaining them under pressure.

Methodology Applied
Scientific EffectOsmotic pressure: Osmotic Pressure

Implementation Method 2

superabsorbents or superabsorbent compositions, their application and their production are given by F. L. Buchholz and A. T. Graham (editors) in 'Modern Superabsorbent Polymer Technology'

Methodology Applied
Scientific EffectHydrogel formation: Hydrogel

Implementation Method 3

the superabsorbent/hydrogel's ability to effectively absorb the liquid during swelling and distribute it throughout the gel layer

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 4

distribute it throughout the gel layer, while minimizing the amount of unbound urine in the diaper

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP2773691B1Superabsorbent polymers for highly filled and fiber-free hygiene products
Publication Date: 2020.07.15 EVONIK SUPERABSORBER GMBH
  • EP2773691B1 patent drawingFigure 1
  • EP2773691B1 patent drawingFigure 2
  • EP2773691B1 patent drawingFigure 3

AI summary

The invention relates to a particulate, absorbent polymer material comprising at least one of the following properties: i) a maximum APCi x 10 sec-value of >=1.6 for at least one number i selected from the group of the whole numbers from 2 to 12 (=APCmax); ii) a value for the sum of all APCi × 10 sec-values of >= 12 for all numbers i from the group of whole numbers from 2 to 12 (=APCsum); wherein the APCi x 10 sec-value is defined as follows: APCi × 10 sec=QIi × 10 sec-value2 ×PIi × 10 sec-value, wherein - the QIi x 10 sec-value value is the value of the source index determined according to the test method described herein i x 10 seconds after adding the 0.9 wt % of NaCl solution and - the PIi x 10 sec-value the value of the permeability index according to the test method described herein i x 10 seconds after adding the 0.9 wt % of NaCl solution. The invention also relates to an absorbent core comprising such a particulate absorbent material, to a hygiene product, to a method for producing an absorbent core and to an absorbent core that can be obtained by said method.