Superabsorbent Polymer Nanoparticle Silane Crosslinking

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Solution Overview

Problem

Current superabsorbent polymers with high swelling capacity often have a fragile structure and inadequate mechanical resistance, leading to insufficient fluid absorption and rapid fluid release, which is not suitable for various applications requiring both high absorption and retention capabilities.

Innovation Solution

A polymer matrix-based superabsorbent material comprising nanoparticles with a size range of 0.1-500 nanometers, water-soluble monomers suitable for radical polymerization, and vinyl alkoxysilane derivative agents as crosslinkers, which enhances swelling capacity, mechanical strength, and controlled fluid release.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If crosslinking density is increased to improve mechanical properties, then gel strength is improved, but swelling capacity decreases

Engineering Contradiction:
Improvegel strengthVSAvoidswelling capacity
Core Design Contradiction:
StrengthVSQuantity of substance

Solution Approach 1:

The patent changes the chemical parameters of the crosslinking agent by using vinyl alkoxysilane derivatives with different alkoxy groups (methoxy, ethoxy, propoxy) and varying carbon chain lengths. This allows optimization of the balance between gel strength and swelling capacity by selecting specific crosslinking agents that provide adequate mechanical properties while maintaining sufficient fluid absorption capability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite polymeric structure by combining acrylic acid or acrylamide monomers with vinyl alkoxysilane derivative crosslinking agents. This composite approach allows the material to exhibit both the hydrophilic swelling properties of the acrylic/acrylamide backbone and the mechanical strengthening effects of the silane crosslinking network.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If swelling capacity is increased to improve fluid absorption, then fluid absorption capacity is improved, but mechanical resistance deteriorates

Engineering Contradiction:
Improvefluid absorption capacityVSAvoidmechanical resistance
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent optimizes the swelling capacity parameter by controlling the monomer-to-crosslinker ratio and selecting specific vinyl alkoxysilane derivatives with varying hydrophobicity. The alkoxy group type and chain length are adjusted to achieve the desired balance between fluid absorption and structural integrity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces local quality variations by using crosslinking agents with different alkoxy chain lengths and types, creating regions of varying crosslinking density and hydrophobicity within the polymer matrix. This allows different parts of the material to perform different functions - some regions optimized for absorption, others for structural support.

Inventive Principle:
Principle #3Local quality

3Stability of the object's composition

If crosslinking density is increased to improve gel strength, then structural stability is improved, but fluid release rate increases

Engineering Contradiction:
Improvestructural stabilityVSAvoidfluid retention time
Core Design Contradiction:
Stability of the object's compositionVSDuration of action of moving object

Solution Approach 1:

The patent controls the fluid release rate by adjusting the crosslinking density parameters through selection of specific vinyl alkoxysilane derivatives. The alkoxy group type and chain length are optimized to achieve moderate crosslinking that provides structural stability while maintaining controlled fluid release characteristics.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The vinyl alkoxysilane derivative acts as an intermediary crosslinking agent that mediates between the hydrophilic polymer chains and provides moderate structural support. The alkoxy groups serve as intermediaries that can be tuned to achieve the desired balance between structural stability and fluid retention.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The material achieves improved swelling capacity, mechanical strength, and prolonged fluid retention, addressing the limitations of existing superabsorbent polymers by maintaining structure under pressure and releasing fluid slowly, suitable for agricultural, horticultural, and industrial applications.

Implementation Method 1

superabsorbent polymers are preferred due to their water retention properties. Superabsorbent polymers (SAP) are cross-linked, water-insoluble, hydrophilic synthetic materials that can absorb fluids hundreds of times their own weight.

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

The crosslinking density of the polymeric structure with super absorbent characteristics directly affects the fluid absorption capacity and gel strength of said polymeric structure.

Methodology Applied
Scientific EffectChemical Bonding: Chemical Bonding

Implementation Method 3

Superabsorbent polymers (SAP) are cross-linked, water-insoluble, hydrophilic synthetic materials

Methodology Applied
Scientific EffectCross-linking:

Implementation Method 4

A polymer matrix based superabsorbent material comprising nanoparticles with a particle size in the range of 0.1-500 nanometers, one or more water-soluble monomers suitable for radical polymerization, and at least one vinyl alkoxysilane derivative agent as a crosslinker.

Methodology Applied
Scientific EffectRadical polymerization: Photopolymerisation

Data Source

PatentUS20230114465A1Polymer matrix based superabsorbent material
Publication Date: 2023.04.13 SABANCI UNIVERSITY

AI summary

A polymer matrix based superabsorbent material is provided, which is made of a polymer including nanoparticles with a particle size in the range of 0.1-500 nanometers, one or more water-soluble monomers suitable for radical polymerization, and at least one vinyl alkoxysilane derivative agent as a crosslinker. A method of producing the polymer matrix based superabsorbent material is also provided, which includes steps of: obtaining a solution by adding a solvent to the one or more water-soluble monomers suitable for the radical polymerization, obtaining a reaction mixture by adding the at least one vinyl alkoxysilane derivative agent as the crosslinker to the solution, adding the nanoparticles with the particle size in the range of 0.1-500 nanometers to the reaction mixture, and obtaining the polymer by a polymerization process.