Solid Superacid Separator Coating for Lithium Dendrite Suppression

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Solution Overview

Problem

Lithium metal secondary batteries face issues with lithium dendrite growth, uneven reaction distribution, and irreversible chemical reactions at the interface between the lithium electrode and electrolyte, leading to reduced stability, lifespan, and energy density.

Innovation Solution

A solid superacid coating layer with a porous structure, comprising sulfated zirconia, is applied to the separator or lithium metal negative electrode, enhancing lithium ion mobility and reaction uniformity, suppressing dendrite growth and irreversible reactions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If lithium metal is used as the negative electrode to achieve high energy density, then the specific capacity increases significantly, but lithium dendrites grow on the electrode surface causing short circuits and safety issues

Engineering Contradiction:
Improvespecific capacityVSAvoidsafety
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

A solid superacid coating layer is introduced as an intermediary between the lithium metal negative electrode and the electrolyte solution. This coating layer mediates the interaction by providing a controlled interface that allows lithium ion transport while preventing direct contact between lithium metal and electrolyte, thereby suppressing dendrite growth and eliminating safety hazards associated with dendrite-induced short circuits

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If a coating film is applied to suppress lithium dendrites physically, then dendrite growth is inhibited, but the method cannot fundamentally control unidirectional growth and lithium loss occurs

Engineering Contradiction:
Improvedendrite suppressionVSAvoidlithium loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The solid superacid coating layer fundamentally changes the interfacial parameters between lithium metal and electrolyte. By modifying the chemical and physical properties of the interface, the coating enables uniform lithium ion flux distribution and controlled deposition, transforming the unidirectional dendritic growth into uniform plating that prevents lithium loss

Inventive Principle:
Principle #35Parameter changes

3Reliability

If the SEI characteristics are enhanced through electrolyte improvement, then protective film formation is improved, but mechanical properties remain low and effects reduce in later cycles due to consumptive reactions

Engineering Contradiction:
Improveprotective film formationVSAvoidcycle stability
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

Instead of attempting to improve the entire electrolyte system, the solid superacid coating is applied locally at the critical lithium metal-electrolyte interface. This localized modification provides the necessary protective function exactly where needed, creating a stable interface that maintains its effectiveness throughout cycling without the consumptive reactions that plague bulk electrolyte modifications

Inventive Principle:
Principle #3Local quality

4Manufacturing precision

If three-dimensional current collectors are used to achieve homogeneous lithium deposition, then charge distribution is controlled, but irreversible surface chemical reactions between lithium and electrolyte increase causing lithium and electrolyte loss

Engineering Contradiction:
Improvedeposition uniformityVSAvoidlithium and electrolyte loss
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The solid superacid coating serves as an intermediary layer that decouples the function of uniform lithium deposition from direct lithium-electrolyte contact. The coating allows homogeneous charge distribution to be achieved while simultaneously blocking the pathway for irreversible chemical reactions, thus preventing both lithium and electrolyte loss

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solid superacid coating layer improves mechanical properties, prevents lithium loss, and achieves high energy density and extended lifespan by controlling lithium dendrite growth and uniform reaction processes.

Implementation Method 1

improving the mobility and the reaction uniformity of lithium at an interface of the lithium metal negative electrode and an electrolyte solution

Methodology Applied
Scientific EffectIon mobility enhancement:

Implementation Method 2

capable of suppressing a growth of lithium dendrites in a lithium metal secondary battery

Methodology Applied
Scientific EffectDendrite suppression:

Implementation Method 3

A solid superacid coating layer with a porous structure, comprising sulfated zirconia, is applied to the separator or lithium metal negative electrode

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3723161B1Separator, lithium metal negative electrode, and lithium metal secondary battery having solid superacid coating layer
Publication Date: 2024.11.20 KOREA ELECTRONICS TECH INST
  • EP3723161B1 patent drawingFigure 1~2
  • EP3723161B1 patent drawingFigure 3
  • EP3723161B1 patent drawingFigure 4~5

AI summary

The present disclosure provides a separator, a lithium metal negative electrode, and a lithium metal secondary battery which include a solid superacid coating layer. The solid superacid coating layer suppresses a growth of lithium dendrites in a lithium metal secondary battery employing lithium metal as a negative electrode by improving a mobility and a reaction uniformity of lithium at an interface of the lithium metal negative electrode and an electrolyte solution. In the lithium metal secondary battery, the solid superacid coating layer comprising solid superacid material having a porous structure is formed on at least one of the lithium metal negative electrode and the separator.