Nickel-Based Superalloy Composition Tuning for Crack-Free SLM

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Solution Overview

Problem

Nickel-based superalloys fabricated by selective laser melting (SLM) are prone to cracking due to rapid cooling rates, repeated remelting, and large thermal gradients, which result in residual stress and deformation.

Innovation Solution

The method involves reducing the content of elements Zr and B, which form low melting point phases, and adjusting the total content of (Ti+Al) to 4.5 wt % or below, while controlling specific SLM process parameters such as substrate heating temperature, rotation angle, laser power, scanning speed, and powder layer thickness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional SLM process parameters are used, then the manufacturing process can be completed, but cracking occurs in the as-built part

Engineering Contradiction:
Improvemanufacturing efficiencyVSAvoidcrack-free quality
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies parameter changes by systematically optimizing SLM process parameters including laser power (200-400W), scanning speed (200-800mm/s), hatching space (0.05-0.15mm), and substrate temperature (50-200℃) to eliminate cracking while maintaining manufacturing efficiency. The patent also changes alloy composition parameters by controlling content of alloying elements to prevent low melting point phase formation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies local quality by implementing different scanning strategies (unidirectional, bidirectional, spiral, meander) for different regions of the part, and using localized heat treatment processes to address residual stress and cracking susceptibility in specific areas. The support structure design also varies locally to prevent deformation in critical regions

Inventive Principle:
Principle #3Local quality

2Reliability

If alloy composition is optimized to prevent cracking, then crack resistance improves, but alloy design complexity increases

Engineering Contradiction:
Improvecrack resistanceVSAvoidalloy composition control
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent establishes specific compositional parameter ranges: Cr (5-20%), Co (5-15%), Mo (2-5%), W (1-3%), Al (2-5%), Ti (2-5%), and limiting Zr to 0.01-0.10% and B to 0.01-0.05%. These parameter specifications provide clear guidance for alloy design and manufacturing while ensuring crack resistance through prevention of low melting point phase formation

Inventive Principle:
Principle #35Parameter changes

3Speed

If rapid cooling rate is used in SLM, then layer-by-layer building speed increases, but residual stress and deformation increase

Engineering Contradiction:
Improvebuilding speedVSAvoidresidual stress
Core Design Contradiction:
SpeedVSStress or pressure

Solution Approach 1:

The patent applies preliminary action by preheating the substrate to 50-200℃ before deposition, which reduces the thermal gradient between the laser-melted region and the bulk material. This preliminary thermal preparation prevents excessive residual stress and deformation while maintaining rapid cooling rates for high building speed

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent optimizes the balance between scanning speed (200-800mm/s) and laser power (200-400W) to control the cooling rate. By adjusting these parameters, the process achieves sufficiently rapid cooling for layer-by-layer building while avoiding excessively high cooling rates that would cause thermal shock and cracking

Inventive Principle:
Principle #35Parameter changes

4Productivity

If high laser power is used, then melting efficiency increases, but thermal gradient and cracking susceptibility increase

Engineering Contradiction:
Improvemelting efficiencyVSAvoidcrack susceptibility
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent establishes an optimized range for laser power (200-400W) and scanning speed (200-800mm/s) that balances melting efficiency with thermal gradient control. This parameter optimization ensures sufficient energy input for complete powder melting while maintaining a thermal gradient that prevents cracking by avoiding excessive heat accumulation

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively prevents cracking in SLM-built nickel-based superalloys, resulting in parts with high density, no crack defects, and excellent mechanical properties, including a tensile strength of up to 1145 MPa at room temperature.

Implementation Method 1

The SLM technology directly melts metal powder layer by layer using high-energy laser beam based on three-dimensional computer-aided design data

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 2

the rapid cooling rate, repeated remelting and large thermal gradient in the SLM process could lead to a large residual stress in the as-built part

Methodology Applied
Scientific EffectRapid cooling: Cooling

Data Source

PatentUS12214422B2Method for preventing cracking of nickel-based superalloy fabricated by selective laser melting
Publication Date: 2025.02.04 CENT SOUTH UNIV

AI summary

A method for preventing cracking of nickel-based superalloy fabricated by selective laser melting (SLM) belongs to the field of additive manufacturing (AM). The method of preparing an as-built part with a high density, no crack defects, and good mechanical properties includes: reducing the content of elements Zr and B forming low melting point phase in a nickel-based superalloy, adjusting the total content of Al and Ti in the alloy to 4.5 wt % or below, and combining with the control of special SLM process parameters. The new method has the advantages of a reasonable component design, a simple preparation process, and good performance of the as-built part, and therefore is suitable for large-scale application.