Superalloy Grain Growth Control via Refractory Conduits

Solution Overview

Problem

Current superalloy casting practices face challenges in managing grain growth during solidification, particularly in achieving consistent grain size and microstructure, as existing methods like agitation, inoculation, and low pouring temperature are complex and introduce defects such as microporosity and non-metallic inclusions.

Innovation Solution

The method involves selectively arranging refractory conduits with heating or cooling elements in the superalloy melt to induce a temperature gradient, controlled by a controller to manage grain growth, promoting directional grain growth and improving the consistency of castings.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If agitation is used to break up dendrites and increase nucleation sites, then grain growth is controlled, but microporosity is introduced requiring post cast hot isostatic pressing

Engineering Contradiction:
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

A refractory conduit is introduced as an intermediary element between the mold wall and the melt. The conduit acts as a thermal mediator that creates a controlled temperature gradient, enabling directional grain growth without requiring mechanical agitation that would create pores. The conduit wall serves as a nucleation site while maintaining structural integrity.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The mechanical agitation method is replaced with a thermal field-based approach. Instead of mechanically stirring the melt to control grain growth, the patent uses a refractory conduit to create a temperature gradient that passively directs solidification, eliminating the need for mechanical intervention and subsequent pore-closing operations.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If inoculation with compounds of lower melting point is used to increase nucleation sites, then grain growth is inhibited, but non-metallic inclusions are introduced which can initiate fatigue cracks

Engineering Contradiction:
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The refractory conduit serves as a clean intermediary structure that provides nucleation sites without introducing foreign compounds. The conduit wall, being refractory material, creates a controlled thermal interface that promotes grain growth control while avoiding the contamination issues associated with chemical inoculants.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Instead of using chemical compounds to modify grain growth, the patent uses a physical template (the refractory conduit) that replicates the desired grain structure. The conduit geometry and thermal properties are designed to produce the target microstructure through passive thermal field interaction, avoiding chemical addition.

Inventive Principle:
Principle #26Copying

3Manufacturing precision

If low pouring temperature is maintained to promote fast freeing and inhibit grain growth, then grain growth is controlled, but the process becomes complex and relatively inflexible

Engineering Contradiction:
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The thermal field is segmented into distinct zones using the refractory conduit. The conduit creates a localized thermal barrier that segments the melt into different temperature regions, enabling independent control of grain growth in specific areas without requiring complex overall process control.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent changes the thermal parameters locally by introducing the refractory conduit with specific thermal conductivity properties. This local parameter change creates the desired temperature gradient without requiring changes to the overall pouring temperature or process parameters, maintaining flexibility.

Inventive Principle:
Principle #35Parameter changes

4Manufacturing precision

If very slow extractions of the solidified part from the hot zone are used for large directional or single crystal grain control, then grain growth is controlled, but the process becomes complex and relatively inflexible

Engineering Contradiction:
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The refractory conduit is positioned in the mold before the melt is poured. This preliminary arrangement pre-establishes the thermal field configuration that will guide grain growth during solidification, eliminating the need for slow extraction or complex post-cast adjustments.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The refractory conduit acts as a thermal intermediary that mediates between the hot zone and the melt. It creates a controlled thermal interface that directs solidification without requiring mechanical extraction control, simplifying the overall process while maintaining grain growth precision.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for precise control of grain growth direction and speed, enhancing the quality and consistency of superalloy castings by minimizing defects and simplifying the process, while maintaining flexibility in the solidification process.

Implementation Method 1

adjustment of a temperature of the heating wire of the heating element or a flow-rate of the coolant of the cooling element to induce a temperature gradient in the superalloy melt

Methodology Applied
Scientific EffectTemperature gradient: Temperature Gradient

Implementation Method 2

selectively arranging one or more refractory conduits in the superalloy melt... refractory conduits may be a heating element and/or a cooling element

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentUS10105757B2Grain growth management system and methods of using the same
Publication Date: 2018.10.23
  • US10105757B2 patent drawing
  • US10105757B2 patent drawing
  • US10105757B2 patent drawing

AI summary

System, methods for improving grain growth in a cast melt of a superalloy are provided. The system includes at least a mold having a shape defining a part of a turbo machine, e.g., a turbine blade. A cast melt, e.g., a superalloy, is poured into the mold, and one or more heating/cooling elements are arranged in the cast melt. The system further includes a controller operatively connected to the elements for controlling the electrical current of, e.g., a heating wire of the heating element, or controlling the flow-rate for, e.g., a coolant of the cooling element. By controlling, i.e., adjusting the current and/or flow-rate, via the controller, a temperature gradient may be induced to improve grain growth.