Electron Beam Melted Superalloys With Seeded Texture Control

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Solution Overview

Problem

Current rapid prototyping and additive-layer manufacturing techniques lack control over the microstructure of metal formations, leading to lower moduli and increased wear, particularly in nickel-based superalloy products.

Innovation Solution

A process involving electron beam melting of a metal alloy powder composition in the presence of a seed crystal to achieve highly textured or single crystal microstructures, with optional use of inoculants and subsequent heat treatment or hot isostatic pressing to control the microstructure and enhance properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If rapid prototyping or additive-layer manufacturing techniques are used to fabricate metal products, then complex shapes can be achieved, but the microstructure of the metal formations cannot be controlled

Engineering Contradiction:
Improvecomplex shape fabricationVSAvoidmicrostructure control
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

A seed crystal is introduced at the beginning of the electron beam melting process to establish the desired microstructure before the bulk material is formed. This preliminary action of nucleation control allows the subsequent additive manufacturing process to produce parts with controlled microstructures while maintaining complex geometries

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention applies different microstructural characteristics to different regions of the part by controlling seed crystal placement and orientation. This allows specific areas to have optimized microstructures for their functional requirements while other areas maintain the complex shape requirements, achieving local quality optimization throughout the part

Inventive Principle:
Principle #3Local quality

2Ease of manufacture

If current rapid prototyping techniques are used without microstructure control, then manufacturing complexity is reduced, but the modulus and wear resistance decrease

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidmodulus and wear resistance
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The invention changes the physical and chemical parameters of the melting process by controlling seed crystal characteristics (size, orientation, composition) and processing conditions (electron beam parameters, heating rates, cooling rates). These parameter changes enable the production of parts with enhanced modulus and wear resistance while maintaining the simplicity of additive manufacturing processes

Inventive Principle:
Principle #35Parameter changes

3Device complexity

If electron beam melting is used without seed crystal, then process simplicity is maintained, but crystallographic texture cannot be controlled

Engineering Contradiction:
Improveprocess simplicityVSAvoidcrystallographic texture control
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The seed crystal serves as an intermediary element that mediates between the simple electron beam melting process and the desired controlled crystallographic texture. This intermediary provides the nucleation sites and orientation templates needed for texture control without requiring complex modifications to the electron beam melting equipment or process

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process enables the production of superalloy metals with controlled crystallographic textures, improving mechanical properties such as ductility and creep resistance, and reducing crystallographic texture, resulting in enhanced performance for aerospace applications.

Implementation Method 1

processing the metal alloy powder composition in the presence of the seed crystal to provide a superalloy metal having a highly textured or single crystal microstructure; and characterised in that the processing step is performed by electron beam melting

Methodology Applied
Scientific EffectElectron beam melting: Electron Beam

Implementation Method 2

providing a seed crystal; processing the metal alloy powder composition in the presence of the seed crystal to provide a superalloy metal having a highly textured or single crystal microstructure

Methodology Applied
Scientific EffectCrystallisation: Crystallisation

Implementation Method 3

the process for the preparation of a superalloy metal according to the invention further comprises subjecting the superalloy metal, after processing, to heat treatment

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 4

the process for the preparation of a superalloy metal according to the invention further comprises subjecting the superalloy metal, after processing, to heat treatment, hot isostatic pressing (HIP), or both

Methodology Applied
Scientific EffectHot isostatic pressing: Hot Isostatic Pressing

Data Source

PatentEP3065901B1Method for preparation of a superalloy having a crystallographic texture controlled microstructure by electron beam melting
Publication Date: 2021.07.14 UNITED TECH CORP
  • EP3065901B1 patent drawingFigure 1
  • EP3065901B1 patent drawingFigure 2
  • EP3065901B1 patent drawingFigure 3a

AI summary

The present disclosure provides a method of preparing superalloy metals having a crystallographic texture controlled micro structure by electron beam melting.