Swirled Flow Chemical Vapor Deposition Reactor

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Solution Overview

Problem

Current chemical vapor deposition techniques face challenges in achieving uniform temperature and precursor gas distribution, leading to non-uniform matrix deposition and increased voids in ceramic matrix composites, which affects their mechanical and thermal properties.

Innovation Solution

A system utilizing a reactor vessel with a heat source and reactor inlets configured to produce a swirling flow of precursor gas around a radially central core region, enhancing temperature uniformity and precursor gas distribution through controlled flow rates, angles, and substrate rotation, thereby optimizing the CVI process for uniform matrix deposition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional chemical vapor deposition techniques are used, then the deposition process can be performed, but uniform temperature and precursor gas distribution cannot be achieved, leading to non-uniform matrix deposition

Engineering Contradiction:
Improveuniformity of matrix depositionVSAvoidtemperature uniformity
Core Design Contradiction:
Manufacturing precisionVSTemperature

Solution Approach 1:

The patent introduces substrate rotation to dynamically change the relative position between the substrate and precursor gas flow, transforming a static deposition process into a dynamic one. This rotation ensures all areas of the substrate receive equivalent exposure to precursor gas over time, achieving uniform matrix deposition despite non-uniform instantaneous gas distribution

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent introduces a swirling flow field as an intermediary mechanism between the precursor gas inlet and the substrate. This swirl flow redistributes the precursor gas uniformly across the reactor chamber before deposition, acting as a mediator that transforms non-uniform gas injection into uniform gas distribution at the substrate surface

Inventive Principle:
Principle #24Intermediary (Mediator)

2Manufacturing precision

If conventional chemical vapor deposition techniques are used, then the deposition process can be performed, but non-uniform matrix deposition occurs, leading to increased voids in ceramic matrix composites

Engineering Contradiction:
Improveuniformity of matrix depositionVSAvoidvoids in composite
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

Substrate rotation dynamically exposes all substrate areas to precursor gas, ensuring complete and uniform matrix infiltration. This eliminates stagnant zones where voids would form, as every area receives adequate precursor gas exposure during the rotation cycle

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The swirling flow field acts as an intermediary that uniformly distributes precursor gas throughout the reactor chamber, preventing localized depletion zones that would lead to void formation. The swirl ensures continuous precursor supply to all substrate surfaces

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If substrate rotation and swirling flow are implemented, then uniform matrix deposition is achieved, but device complexity increases

Engineering Contradiction:
Improveuniformity of matrix depositionVSAvoidcomplexity of reactor system
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The substrate rotation mechanism adds dynamic capability to an otherwise static deposition system. A single rotational degree of freedom provides comprehensive uniformity improvement without requiring complex multi-axis motion systems or sophisticated control mechanisms

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The swirling flow is generated by introducing the gas at an angle through existing inlet structures, utilizing the gas flow itself to create the swirl rather than adding separate mechanical swirl generators. This passive flow control method achieves uniform distribution without adding complex active control systems

Inventive Principle:
Principle #24Intermediary (Mediator)

4Productivity

If conventional deposition methods are used, then the process is simple, but production speed is limited due to non-uniform deposition requiring longer processing times

Engineering Contradiction:
Improveproduction speed of ceramic matrix compositesVSAvoiduniformity of matrix deposition
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

Substrate rotation enables uniform deposition to be achieved more rapidly by ensuring all areas receive equivalent precursor exposure simultaneously during rotation, eliminating the need for extended processing times required by static methods to achieve comparable uniformity

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The swirling flow field accelerates precursor gas distribution throughout the reactor chamber, reducing the time required for uniform matrix deposition. The enhanced convective mixing and uniform gas distribution enable faster infiltration rates while maintaining deposition uniformity

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in faster production of ceramic matrix composites with improved uniformity, reduced voids, and enhanced mechanical properties, suitable for applications in gas turbine engines and other high-performance components.

Implementation Method 1

heating, using a heat source, a reactor vessel

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

The at least one reactor inlet may be configured to produce swirling flow of the precursor gas around the radially central core region of the reactor vessel

Methodology Applied
Scientific EffectSwirling flow: Vortex Ring

Implementation Method 3

Chemical vapor infiltration (CVI), a form of chemical vapor deposition, may be used to deposit ceramic matrix materials for ceramic matrix composites (CMCs)

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Data Source

PatentUS11008652B2Swirled flow chemical vapor deposition
Publication Date: 2021.05.18 ROLLS ROYCE HIGH TEMPERATURE COMPOSITES INC
  • US11008652B2 patent drawing
  • US11008652B2 patent drawing
  • US11008652B2 patent drawing

AI summary

A system may include a reactor vessel comprising an outer wall, a heat source thermally coupled to the reactor vessel, at least one reactor inlet in the outer wall, and at least one reactor outlet. The reactor vessel may be configured to house a porous preform in a radially central core region. The at least one reactor inlet may be configured to introduce a precursor gas to the reactor vessel to produce swirling flow of the precursor gas around the radially central core region of the reactor vessel. The at least one reactor outlet may be configured to remove exhaust gas from the reactor vessel and assist in maintaining a dynamic pressure of the reactor vessel greater than a pressure in the porous preform.