Bifunctional Catalyst for Syngas Conversion

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Solution Overview

Problem

Current methods for converting syngas into liquid fuel, such as the Fischer-Tropsch process, suffer from low selectivity for target products like gasoline and high production of aromatic hydrocarbons, which is environmentally unfavorable.

Innovation Solution

A bifunctional composite catalyst comprising a metal oxide and a zeolite with 1D ten-membered ring porous channels, specifically designed for direct conversion of syngas into liquid fuel, optimizing the reaction conditions to achieve high selectivity for C5-C11 hydrocarbons while minimizing aromatic hydrocarbon production.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If traditional Fischer-Tropsch catalyst is used for direct conversion of syngas, then the process flow is simplified, but the selectivity for gasoline is low and aromatic hydrocarbon content is high

Engineering Contradiction:
Improveprocess flowVSAvoidproduct selectivity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The catalyst is segmented into two distinct functional components: Component A (metal oxide for CO activation) and Component B (zeolite for C-C coupling). This segmentation allows each component to specialize in one function, with Component A activating CO and H2 and Component B performing selective C-C coupling to form gasoline-range hydrocarbons, thereby resolving the contradiction between process simplicity and product selectivity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent uses a composite catalyst system combining metal oxide (Component A) and zeolite (Component B) with specific pore structures (1D ten-membered ring or 3D eight-membered ring). This composite material approach enables the catalyst to simultaneously achieve high gasoline selectivity and low aromatic hydrocarbon content while maintaining a simplified direct conversion process.

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If ZSM-5 zeolite is used to separate CO activation from C-C coupling, then gasoline selectivity is improved, but aromatic hydrocarbon content becomes too high

Engineering Contradiction:
Improvegasoline selectivityVSAvoidaromatic hydrocarbon content
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The patent applies local quality by selecting zeolites with specific local pore structure characteristics (1D ten-membered ring or 3D eight-membered ring) that create favorable local environments for linear hydrocarbon formation. These specific pore structures provide localized active sites that promote C-C coupling while suppressing aromatic formation, thereby achieving high gasoline selectivity with low aromatic content.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent changes the structural parameters of the zeolite component, specifically selecting zeolites with 1D ten-membered ring pores (TON, AEL, MTT, MRE topology) or 3D eight-membered ring pores instead of conventional ZSM-5. This parameter change in pore structure fundamentally alters the reaction pathway to favor linear hydrocarbons over aromatic compounds while maintaining gasoline selectivity.

Inventive Principle:
Principle #35Parameter changes

3Device complexity

If direct conversion of syngas is implemented, then process flow and unit operations are reduced, but product selectivity control is difficult

Engineering Contradiction:
Improveunit operationsVSAvoidtarget product selectivity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by pre-activating CO and H2 on Component A (metal oxide) before they reach Component B (zeolite). This preliminary activation creates surface carbon species and hydrogen species in optimal proportions, which then undergo selective C-C coupling on Component B to form gasoline-range hydrocarbons. This preliminary action ensures high selectivity even in the simplified direct conversion process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The bifunctional catalyst acts as an intermediary system where Component A (metal oxide) and Component B (zeolite) work sequentially. Component A serves as an intermediary that activates syngas and transfers activated species to Component B, which then performs the selective C-C coupling. This intermediary mechanism enables precise control of product selectivity while maintaining process simplicity.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst achieves a selectivity of 50-80% for liquid fuel with reduced aromatic hydrocarbon content and low methane side product, simplifying the process and reducing energy consumption.

Implementation Method 1

CO and H2 molecules are dissociated and absorbed on the surface of the catalyst to produce surface C atoms and O atoms

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

The bifunctional catalyst composed of oxides and zeolites can be used to separate CO activation from C—C coupling at two active centers

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

The C atoms and the O atoms react with hydrogen absorbed on the surface of the catalyst to form a methylene (CH2) intermediate while releasing water molecules

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentUS11999910B2Catalyst and method for preparing low aromatic hydrocarbon liquid fuel through direct conversion of syngas
Publication Date: 2024.06.04 DALIAN INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

AI summary

A method for preparing liquid fuel by direct conversion of syngas uses the syngas as reaction raw material and conducts a catalytic conversion reaction on a fixed bed or a moving bed. The catalyst is a composite catalyst formed by compounding component I and component II in a mechanical mixing mode. The active ingredient of the component I is a metal oxide, and the component II is at least one of zeolites with one-dimensional ten-membered ring porous channels; and a weight ratio of the active ingredient in the component I to that in the component II is 0.1-20. The reaction process has high product yield and selectivity. The selectivity for liquid fuel composed of C5-C11 can reach 50-80%. The selectivity for aromatic hydrocarbon is less than 40% in C5-C11, while the selectivity for methane side product is less than 15%.