Tannic Acid Coating for Silicon Anodes Under Volume Expansion

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Silicon-based negative electrode active materials in secondary batteries are prone to breaking due to volume expansion during charging and discharging, leading to reduced lifespan and performance.

Innovation Solution

A composition comprising tannic acid and a tris buffer solution is used to form cross-linked tannic acid-based coating films on primary particles of a silicon-based negative electrode active material, creating secondary particles through agglomeration and crosslinking, thereby reducing volume expansion.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon-based negative electrode active material is used to increase theoretical capacity, then capacity increases, but volume expansion occurs during lithium intercalation

Engineering Contradiction:
Improvetheoretical capacityVSAvoidvolume expansion
Core Design Contradiction:
Quantity of substanceVSVolume of moving object

Solution Approach 1:

The patent applies the nesting principle by forming a coating film on the surface of silicon-based negative electrode active material particles. The coating film acts as an outer layer that encapsulates the silicon core, allowing the high-capacity silicon material to be utilized while the coating layer accommodates and buffers the volume expansion during lithium intercalation, preventing direct mechanical damage to the electrode structure.

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The patent employs a coating film that functions as a flexible shell around the silicon-based active material. This thin film structure allows it to deform elastically during volume expansion and contraction cycles, maintaining structural integrity and preventing particle breakage while still enabling lithium ion transport to the silicon core.

Inventive Principle:
Principle #30Flexible shells and thin films

2Quantity of substance

If silicon volume increases by up to 300% due to lithium intercalation, then capacity is achieved, but negative electrode breaks and cycling characteristic deteriorates

Engineering Contradiction:
ImprovecapacityVSAvoidcycling characteristic
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies beforehand cushioning by pre-forming a coating film on the silicon-based negative electrode active material before electrode assembly. This coating film serves as a cushioning layer that absorbs and distributes the mechanical stress generated during volume expansion, preventing direct transmission of stress to the electrode binder and current collector, thereby maintaining electrode integrity throughout cycling.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Solution Approach 2:

The patent utilizes composite materials by combining silicon-based active material with a coating film material that has complementary properties. The composite structure leverages the high capacity of silicon while the coating film provides mechanical strength, flexibility, and stability, creating a material system that exhibits both high capacity and excellent cycling characteristics.

Inventive Principle:
Principle #40Composite materials

3Reliability

If coating film is formed to control volume expansion, then electrode integrity is maintained, but manufacturing process complexity increases

Engineering Contradiction:
Improveelectrode integrityVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies self-service by utilizing a coating formation process that leverages the inherent properties of the coating materials and the silicon surface. The coating film forms through self-assembly or spontaneous chemical reactions between the coating precursors and the silicon surface, eliminating the need for complex external equipment or multi-step deposition processes, thereby simplifying manufacturing while ensuring uniform coverage and adhesion.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The tannic acid-based coating film effectively controls volume expansion and prevents damage to the negative electrode active material, enhancing the resistance and lifespan characteristics of the secondary battery.

Implementation Method 1

crosslinks between tannic acid-based coating films

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 2

secondary particles of agglomerated primary particles

Methodology Applied
Scientific EffectAgglomeration: Coagulation

Implementation Method 3

effectively controls volume expansion and prevents damage to the negative electrode active material

Methodology Applied
Scientific EffectVolume expansion control: Physical Containment

Data Source

PatentEP3767712B1Composition for coating a negative electrode active material, negative electrode active material and negative electrode for lithium secondary battery including the same
Publication Date: 2025.01.29 LG ENERGY SOLUTION LTD
  • EP3767712B1 patent drawingFigure 1
  • EP3767712B1 patent drawingFigure 2
  • EP3767712B1 patent drawing

AI summary

The present invention relates to a composition for coating a negative electrode active material, a negative electrode active material for a secondary battery, a negative electrode containing the same, and a lithium secondary battery containing the negative electrode. Particularly, a composition for coating a negative electrode active material, which includes tannic acid, a negative electrode active material for a secondary battery whose surface is coated with a tannic acid-based coating film, a negative electrode for a secondary battery, which includes the negative electrode active material, and a lithium secondary battery including the negative electrode may reduce volume expansion and prevent damage in charging/discharging of the negative electrode active material. Therefore, the secondary battery including the negative electrode of the present invention ultimately improves resistance and life span characteristics.