TEM Sample Preparation for DRAM Trench Capacitors

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Solution Overview

Problem

Conventional TEM sample preparation methods struggle to produce accurate images of small device features in integrated circuits, such as deep trench capacitor structures in DRAM devices, due to difficulties in achieving uniform sample thickness and precise control of ion beam angles, leading to incomplete or distorted observations.

Innovation Solution

A method involving the removal of slices from integrated circuit chips in a directional manner normal to the elongated structures, ensuring a substantially uniform sample thickness, allowing for effective TEM imaging of high aspect ratio structures like deep trench capacitors, which includes capturing images using a transmission electron microscope.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of stationary object

If conventional TEM sample preparation methods are used, then sample thickness can be reduced, but uniformity of sample thickness deteriorates

Engineering Contradiction:
Improvesample thicknessVSAvoiduniformity of sample thickness
Core Design Contradiction:
Length of stationary objectVSManufacturing precision

Solution Approach 1:

The method performs preliminary orientation of the sample before thinning. The sample is first oriented with its surface substantially perpendicular to the elongated structures using ion beam milling, then thinning is performed in a direction substantially parallel to the elongated structures. This preliminary orientation ensures that subsequent thinning produces uniform thickness across the high aspect ratio structures.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention changes the dimension of the ion beam milling action by performing thinning in a direction substantially parallel to the elongated structures rather than perpendicular to them. This dimensional change allows the ion beam to traverse the full length of high aspect ratio structures, ensuring uniform thickness throughout the entire structure length.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Length of stationary object

If conventional ion beam milling is used, then sample thickness can be controlled, but precision of ion beam angle control deteriorates

Engineering Contradiction:
Improvesample thicknessVSAvoidion beam angle control
Core Design Contradiction:
Length of stationary objectVSMeasurement precision

Solution Approach 1:

The method performs preliminary orientation of the sample before thinning. The sample is first oriented with its surface substantially perpendicular to the elongated structures using ion beam milling, then thinning is performed in a direction substantially parallel to the elongated structures. This preliminary orientation ensures that subsequent thinning produces uniform thickness across the high aspect ratio structures.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The elongated structures themselves serve as reference features for determining the correct thinning direction. By aligning the thinning direction parallel to these visible structures, the sample provides its own geometric reference, eliminating the need for precise external angle measurement and control equipment.

Inventive Principle:
Principle #25Self-service

3Reliability

If sample thickness is reduced for TEM imaging, then imaging capability is improved, but observation completeness deteriorates

Engineering Contradiction:
Improveimaging capabilityVSAvoidobservation completeness
Core Design Contradiction:
ReliabilityVSLoss of information

Solution Approach 1:

The invention changes the dimension of the ion beam milling action by performing thinning in a direction substantially parallel to the elongated structures rather than perpendicular to them. This dimensional change allows the ion beam to traverse the full length of high aspect ratio structures, ensuring uniform thickness throughout the entire structure length.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The method ensures that different regions of the sample, particularly the top and bottom portions of high aspect ratio structures, receive equivalent thinning treatment. By milling parallel to the structures, both ends of the structures are uniformly thinned to the same thickness, providing complete and consistent observation throughout the entire structure.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances the resolution and accuracy of TEM analysis for integrated circuits, enabling clear imaging of complex structures without requiring substantial modifications to conventional equipment or processes, thereby improving the manufacturing process for semiconductor devices.

Implementation Method 1

removing a slice of the integrated circuit chip from a portion of the thickness in a directional manner normal to the structure length

Methodology Applied
Scientific EffectIon beam milling: Ion Beam

Data Source

PatentUS7923683B2Method for treatment of samples for transmission electron microscopes
Publication Date: 2011.04.12 SEMICON MFG INT (SHANGHAI) CORP
  • US7923683B2 patent drawing
  • US7923683B2 patent drawing
  • US7923683B2 patent drawing

AI summary

A method for analyzing a sample for the manufacture of integrated circuits, e.g., dynamic random access memory devices, commonly called DRAMS. The method also provides an integrated chip including a thickness, a width, and a length. In a specific embodiment, the integrated chip has at least one elongated structure through a portion of the thickness, while being normal to the width and the length. In a specific embodiment, the elongated structure has a structure width and a structure length that extends through a vertical portion of the thickness. The method includes removing a slice of the integrated chip from a portion of the thickness in a directional manner normal to the structure length. In a specific embodiment, the slice is provided through an entirety of the one elongated structure along the structure length to cause a portion of a thickness of the slice providing the elongated structure to be of a substantially uniform sample thickness. The method also includes capturing one or more images through a portion of the slice using a transmission electron microscope.