Textile Decoloring Using Anionic Polyelectrolytes in Alkaline Solution

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Solution Overview

Problem

Existing textile recycling processes face inefficiencies and complexity in decoloring textile materials, particularly when dealing with both dyed and pigmented materials.

Innovation Solution

A method involving treatment of textile materials in an alkaline solution containing one or more anionic polyelectrolytes, such as carboxymethyl cellulose (CMC), at elevated temperatures for a minimum of 10 minutes, effectively decoloring both dyed and pigmented textiles.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional decoloring processes are used, then textile materials can be decolored, but the process is either not efficient or involves several process steps and chemicals making the recycling process complex

Engineering Contradiction:
Improvedecoloring efficiencyVSAvoidprocess complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent combines decoloring and fiber separation functions into a single treatment step using one alkaline solution containing CMC and NaOH, eliminating the need for separate decoloring and separation processes. This integration directly reduces process complexity while maintaining high decoloring efficiency.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The alkaline solution with CMC serves multiple functions simultaneously: it acts as a decoloring agent for both dyed and pigmented textiles, a separating medium for different fiber types, and a treatment medium that can be reused. This multi-functionality resolves the contradiction by achieving efficient decoloring without adding process steps.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Adaptability or versatility

If conventional decoloring methods are applied, then textile materials can be treated, but the process does not effectively handle both dyed and pigmented materials simultaneously

Engineering Contradiction:
Improveapplicability to different textile typesVSAvoiddecoloring efficiency
Core Design Contradiction:
Adaptability or versatilityVSProductivity

Solution Approach 1:

The patent uses specific parameter combinations (pH 12-14, temperature 80-200°C, CMC concentration 0.1-5%) that create optimal conditions for decoloring both dyed and pigmented textiles. The strong alkaline environment combined with CMC's chelating ability allows universal effectiveness across different textile types while maintaining high decoloring efficiency.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

CMC acts as an intermediary substance that facilitates decoloring through its chelating properties, binding to metal ions in both dye and pigment molecules. This intermediary mechanism enables the solution to effectively treat diverse textile colorings without requiring different process conditions.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If multiple process steps and chemicals are used for decoloring, then thorough decoloring can be achieved, but the recycling process becomes complex

Engineering Contradiction:
Improvedecoloring completenessVSAvoidnumber of process steps
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent merges decoloring chemicals (CMC and NaOH) and functions into a single treatment bath, achieving complete decoloring without requiring multiple sequential steps. The synergistic interaction between CMC's chelating action and NaOH's alkaline environment provides thorough decoloring in one step.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The treatment solution is a composite system combining CMC (a polysaccharide with chelating groups) and NaOH (a strong base). This composite chemical system provides multiple decoloring mechanisms simultaneously, achieving complete decoloring while simplifying the process to a single step.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method significantly improves decoloring efficiency, allowing for simultaneous decoloring and separation of cellulosic and polyester fibers, thus simplifying the recycling process.

Implementation Method 1

the presence of an anionic polyelectrolyte in the alkaline solution, such as carboxymethyl cellulose (CMC), significantly improves decoloring of textile materials

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

treating the textile material in the alkaline solution during a treatment period of at least 10 minutes at a temperature in the range of from 100°C to 180°C

Methodology Applied
Scientific EffectComplexation:

Implementation Method 3

separation of cellulosic material from polyester material

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 4

By adding an anionic polyelectrolyte, such as CMC, to the alkaline solution of WO2020/013755, separation of cellulosic fibers from polyester fibers as well as decoloring of colored fibers can be carried out simultaneously

Methodology Applied
Scientific EffectSelective dissolution:

Data Source

PatentEP4301570B1Method for decoloring of a textile material
Publication Date: 2025.04.23 SODRA SKOGSAGARNA EKONOMISK FORENING
  • EP4301570B1 patent drawingFigure 1~2
  • EP4301570B1 patent drawingFigure 3~4
  • EP4301570B1 patent drawingFigure 5~6

AI summary

The invention concerns a method for decoloring of a textile material, the method comprising the steps of: providing a textile material; providing an alkaline solution containing one or more anionic polyelectrolytes; treating the textile material in the alkaline solution during a treatment period; and recovering at least some of the textile material from the alkaline solution.