Thermal Analyzer Multilayer Insulation Gas Layer

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Solution Overview

Problem

Existing thermal analyzers face challenges in achieving high baseline reproducibility due to thermal hysteresis caused by delayed temperature changes in solid heat insulation materials, leading to fluctuations in the temperature environment around the furnace, which complicates temperature control and limits measurement reliability.

Innovation Solution

A multilayer heat insulation structure is implemented around the furnace, using a gas layer as the interlayer with materials like stainless steel and aluminum, reducing heat capacity and thermal conductivity, allowing for quicker temperature changes and minimizing thermal hysteresis, thereby stabilizing the temperature environment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If solid heat insulation materials are used around the furnace, then heat insulation effect is improved, but thermal hysteresis increases due to delayed temperature changes

Engineering Contradiction:
Improveheat insulation effectVSAvoidbaseline reproducibility
Core Design Contradiction:
Loss of energyVSReliability

Solution Approach 1:

The patent replaces solid heat insulation materials with a gas-filled vacuum chamber structure. The vacuum chamber uses gas (or vacuum) as the heat insulation medium instead of solid materials, which significantly reduces thermal conductivity while minimizing thermal mass. This allows the furnace to reach thermal equilibrium faster and reduces thermal hysteresis during temperature cycling, thereby improving baseline reproducibility while maintaining heat insulation effectiveness.

Inventive Principle:
Principle #29Pneumatics and hydraulics

2Stability of the object's composition

If heat insulation structure with high heat capacity is used, then temperature stability is improved, but temperature response speed deteriorates

Engineering Contradiction:
Improvetemperature stabilityVSAvoidtemperature response speed
Core Design Contradiction:
Stability of the object's compositionVSSpeed

Solution Approach 1:

The vacuum chamber structure uses gas or vacuum as the heat insulation medium, which has extremely low thermal conductivity and minimal heat capacity compared to solid insulation materials. This design maintains temperature stability by preventing heat loss while allowing rapid temperature changes because the gas/vacuum medium does not store significant thermal energy, thus improving temperature response speed without sacrificing stability.

Inventive Principle:
Principle #29Pneumatics and hydraulics

3Loss of energy

If thick solid heat insulation layers are added, then heat insulation performance is improved, but device complexity and size increase

Engineering Contradiction:
Improveheat insulation performanceVSAvoidstructure complexity
Core Design Contradiction:
Loss of energyVSDevice complexity

Solution Approach 1:

The patent employs a vacuum chamber design where the heat insulation function is achieved through the vacuum or gas-filled space itself, eliminating the need for thick solid insulation layers. This approach provides excellent heat insulation performance with minimal structural complexity and compact size, as the vacuum chamber walls serve both structural and insulation purposes simultaneously.

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances baseline reproducibility by reducing thermal hysteresis and maintaining a stable temperature environment, enabling more reliable and consistent thermal analysis across a wide temperature range without the need for complex control systems or structures.

Implementation Method 1

a layer having a heat insulation effect is provided between the layers constituting the wall member. Further, the heat insulation layer is set as a gas layer

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Implementation Method 2

the heat insulation layer is set as a gas layer, and there is used an interlayer material which does not have an excessively high heat capacity as compared to a gas

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Data Source

PatentUS8708556B2Thermal analyzer
Publication Date: 2014.04.29 HITACHI HIGH TECH ANALYSIS CORP
  • US8708556B2 patent drawing
  • US8708556B2 patent drawing
  • US8708556B2 patent drawing

AI summary

A thermal analyzer heats and cools a sample placed inside a furnace for measuring a thermal characteristic of the sample during heating and cooling. The thermal analyzer has a multilayer structure for covering the furnace and its surroundings so as to isolate the furnace and its surroundings from an external environment. The multilayer structure includes a multilayer wall with two layers formed of a material having high thermal conductivity and heat dissipation property. The two layers are spaced apart from one another to provide therebetween an interlayer that contains a substance having a heat capacity substantially equal to a gas contained in the furnace so that heat transfer between the two layers is minimized.