Thermal Barrier Coating Cold Spray Oxidation

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Solution Overview

Problem

Current methods for depositing thermal barrier coatings (TBCs) in gas turbines face challenges in achieving desired porosity while maintaining mechanical strength, and existing chemistries with low thermal conductivity, such as lanthana, are difficult to deposit due to the formation of a glass phase that disrupts the spraying process.

Innovation Solution

A process involving cold spraying a substrate with a feedstock in a region with an oxygen concentration of at least 10%, concurrently oxidizing the substrate, feedstock, and thermal barrier coating, which includes using ceramic particles and a binder to form a thermal barrier coating with graded porosity and increased oxide content, allowing for controlled microstructure and reduced thermal conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If current methods of TBC deposition (EBPVD or APS) are used to increase porosity, then thermal conductivity decreases, but mechanical strength deteriorates

Engineering Contradiction:
Improvethermal conductivityVSAvoidmechanical strength
Core Design Contradiction:
Loss of energyVSStrength

Solution Approach 1:

The invention changes the deposition parameters by using cold spray technology with specific particle velocities and temperatures, along with controlling oxygen concentration during deposition, to achieve a unique microstructure that simultaneously provides high porosity and maintained mechanical strength, resolving the trade-off between thermal insulation and structural integrity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite microstructure within the TBC comprising ceramic particles, metal particles, and oxide phases distributed in a specific configuration. This composite structure achieves both high porosity for thermal insulation and sufficient mechanical strength through the synergistic combination of different material phases

Inventive Principle:
Principle #40Composite materials

2Loss of energy

If TBC chemistry uses low thermal conductivity constituents like lanthana, then thermal insulation improves, but deposition process deteriorates due to glass phase formation

Engineering Contradiction:
Improvethermal conductivityVSAvoiddeposition process
Core Design Contradiction:
Loss of energyVSEase of manufacture

Solution Approach 1:

The invention replaces the conventional thermal-based deposition processes (EBPVD, APS) with cold spray technology, which uses kinetic energy of accelerated particles instead of thermal energy. This substitution avoids the glass phase formation problem that occurs with lanthana-based chemistries in thermal processes, enabling successful deposition of low thermal conductivity materials

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention changes the chemical composition parameters by selecting specific ceramic and metal particle combinations that are compatible with cold spray deposition, avoiding constituents that form problematic glass phases while maintaining low thermal conductivity. The process controls oxygen concentration and particle temperature to achieve desired oxide content without process disruption

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If cold spray is used to deposit TBC, then process control improves, but ceramic retention deteriorates without concurrent oxidation

Engineering Contradiction:
Improveprocess controlVSAvoidceramic retention
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The invention merges the cold spray deposition process with concurrent oxidation by controlling oxygen concentration in the deposition region. This combination allows the metallic binder to oxidize during deposition, creating strong chemical bonds with ceramic particles and improving ceramic retention while maintaining the advantages of cold spray process control

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The invention introduces elevated oxygen concentration (at least 10%) in the deposition region to accelerate oxidation of the metallic binder material during cold spray deposition. This accelerated oxidation enhances ceramic particle retention by creating oxide bridges and strong interfacial bonding between metal and ceramic phases

Inventive Principle:
Principle #38Strong oxidants (Accelerated oxidation)

Data Source

PatentEP2778257B1Process of fabricating thermal barrier coatings
Publication Date: 2017.05.10 GENERAL ELECTRIC CO
  • EP2778257B1 patent drawingFigure 1~2
  • EP2778257B1 patent drawingFigure 3
  • EP2778257B1 patent drawingFigure 4~5

AI summary

A process of fabricating a thermal barrier coating is disclosed. The process includes cold spraying a substrate (101) with a feedstock (402) to form a thermal barrier coating (102) and concurrently oxidizing one or more of the substrate (101), the feedstock (402), and the thermal barrier coating (102). The cold spraying is in a region (103) having an oxygen concentration of at least 10%. In another embodiment, the process includes heating a feedstock (402) with a laser (411) and cold spraying a substrate (101) with the feedstock (402) to form a thermal barrier coating (102). At least a portion of the feedstock (402) is retained in the thermal barrier coating (102). In another embodiment, the process of fabricating a thermal barrier coating includes heating a substrate (101) with a laser (411) and cold spraying the substrate with a feedstock to form a thermal barrier coating.