Thermal Cracking Process for High TAN Crude Oil Conversion

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Solution Overview

Problem

Current methods for processing highly acidic crude oils are inefficient, leading to corrosion issues, costly refining processes, and degradation of crude quality, as they often require special chemicals, complex processes, and frequent use of corrosion inhibitors, and do not effectively convert crude oil into valuable lighter hydrocarbons while minimizing metallurgy changes and corrosion inhibitor usage.

Innovation Solution

A thermal cracking process is employed to convert high TAN crude oils into lighter hydrocarbons, involving desalting, pre-fractionation, thermal reaction, and fractionation, which reduces acidity and removes catalyst poisons like heavy metals, allowing for minimal metallurgy changes and reduced corrosion inhibitor use.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional refining methods are used to process highly acidic crude oil, then the crude oil can be processed, but corrosion of metal surfaces occurs requiring frequent changes of corroded parts or use of expensive refractory metals

Engineering Contradiction:
Improvecrude oil processing capabilityVSAvoidcorrosion of metal surfaces
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and removes the harmful acidic compounds (naphthenic acids) from the crude oil through thermal cracking and fractionation processes. By separating and eliminating these acidic components before the oil enters downstream processing equipment, the corrosion problem is resolved while maintaining processing capability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The thermal cracking process converts the harmful acidic compounds into lighter hydrocarbon products through controlled thermal decomposition. The naphthenic acids are broken down and separated, transforming the harmful substance into useful products while eliminating the corrosion issue.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Reliability

If corrosion inhibitors are used to protect metal surface from corrosion, then metal surface is protected, but the process requires frequent dosing and additional chemical costs

Engineering Contradiction:
Improvemetal surface protectionVSAvoidcorrosion inhibitor dosing system
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent performs preliminary thermal cracking and fractionation to remove acidic compounds before the crude oil contacts metal equipment. This preliminary action eliminates the need for continuous corrosion inhibitor dosing, as the harmful substances are removed upstream in the processing sequence.

Inventive Principle:
Principle #10Preliminary action

3Productivity

If thermal cracking process is used to convert high boiling hydrocarbon to low boiling petroleum, then lighter hydrocarbon products are produced, but acidic compounds remain causing corrosion issues

Engineering Contradiction:
Improvelighter hydrocarbon productionVSAvoidacidic compound content
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent segments the thermal cracking process into multiple stages with intermediate fractionation. The crude oil is cracked into different boiling ranges, then systematically separated into lighter and heavier fractions. This segmentation allows complete removal of acidic compounds from the lighter hydrocarbon products while maintaining production efficiency.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent implements continuous thermal cracking followed by continuous fractionation and separation of acidic compounds. The process maintains continuous operation to ensure complete conversion and separation, eliminating residual acidic compounds while continuously producing lighter hydrocarbon products.

Inventive Principle:
Principle #20Continuity of useful action

4Manufacturing precision

If fractionation column is exposed to acidic crude, then separation is achieved, but costly refining process is required

Engineering Contradiction:
Improveseparation efficiencyVSAvoidrefining process cost
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent performs preliminary thermal cracking to break down complex acidic compounds before they enter the fractionation column. This preliminary action simplifies the separation process, reducing the complexity and cost of the fractionation operation while maintaining high separation efficiency.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process effectively destroys naphthenic acid compounds, reduces acidity, and produces cleaner feedstock for downstream units, eliminating corrosion issues and the need for frequent corrosion inhibitor dosing, while maintaining or improving crude oil quality.

Implementation Method 1

A thermal cracking process is employed to convert high TAN crude oils into lighter hydrocarbons

Methodology Applied
Scientific EffectThermal cracking: Pyrolysis

Implementation Method 2

desalting neat high acidic crude oil to obtain desalted crude

Methodology Applied
Scientific EffectDesalting: Sedimentation

Implementation Method 3

separating the desalted crude in a pre-fractionator column into lighter hydrocarbon material and heavier boiling material

Methodology Applied
Scientific EffectFractionation: Distillation

Data Source

PatentEP3514217B1A process for conversion of high acidic crude oils
Publication Date: 2021.01.06 INDIAN OIL CORP LTD
  • EP3514217B1 patent drawingFigure 1~2

AI summary

The present invention relates to crude oil processing, particularly related to conversion of crude oil containing high amount of naphthenic acid compounds to lighter hydrocarbon materials with minimum capital expenditure. The invented process utilizes a novel scheme for high TAN crude oils by employing thermal cracking process to maximize the residue conversion to valuable products, which require minimum modifications in unit metallurgies and corrosion inhibitor injection schemes in refineries.