Thermoplastic Prepreg Manufacturing via Segmented Heating

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Solution Overview

Problem

The existing methods for manufacturing thermoplastic prepregs result in nonuniform impregnation of fibers due to thermoplastic material creep towards the periphery under heat and pressure, making it unsuitable for high-speed industrial production with controlled mechanical properties and leading to material waste.

Innovation Solution

A method involving heating the complex to a temperature above the melting point of the thermoplastic material without applying pressure initially, followed by applying pressure to enhance impregnation, while preheating and crushing the matrix sheet to reduce thickness and porosity, and using polyethylene terephthalate as the thermoplastic material with multiple reinforcement layers of different fiber orientations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If heat and pressure are applied simultaneously to melt the thermoplastic material for impregnation, then the impregnation process is accelerated, but the thermoplastic material creeps toward the periphery causing nonuniform impregnation

Engineering Contradiction:
Improveimpregnation speedVSAvoidimpregnation uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The process is divided into two distinct stages: first heating without pressure to melt the matrix material uniformly, then applying pressure for impregnation. This segmentation of the heating and pressurization steps prevents the material creep issue while maintaining high productivity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The matrix sheet is preheated to a temperature close to its melting point before being placed in the impregnation tool. This preliminary heating action reduces the temperature difference during subsequent pressurization, minimizing thermal gradients that cause material creep and nonuniform impregnation.

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If high pressure is applied during heating to force impregnation, then impregnation completeness is improved, but material waste increases due to creep toward periphery

Engineering Contradiction:
Improveimpregnation completenessVSAvoidthermoplastic material waste
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The process separates heating and pressurization into sequential steps, allowing complete impregnation without excessive material flow to periphery. This reduces thermoplastic material waste while ensuring thorough fiber impregnation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The matrix sheet undergoes preliminary heating and thickness reduction before impregnation. This pre-treatment ensures optimal material properties for impregnation, reducing the need for excessive pressure that would cause material creep and waste.

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If the matrix sheet is heated to high temperature without pressure, then material creep is prevented, but impregnation efficiency is reduced

Engineering Contradiction:
Improveimpregnation uniformityVSAvoidimpregnation efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The process is segmented into heating phase (without pressure for uniform melting) and pressurization phase (for efficient impregnation). This sequential approach maintains impregnation uniformity while achieving high impregnation efficiency through optimized timing of each step.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The matrix sheet is preliminarily heated to near-melting temperature before pressurization. This preliminary thermal treatment reduces the energy required during pressurization and accelerates the impregnation process, improving overall efficiency while maintaining uniformity.

Inventive Principle:
Principle #10Preliminary action

4Manufacturing precision

If the matrix sheet thickness is reduced to improve impregnation, then impregnation quality is enhanced, but the sheet becomes more fragile and difficult to handle

Engineering Contradiction:
Improveimpregnation qualityVSAvoidsheet handling
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The matrix sheet undergoes preliminary heating and controlled thickness reduction before impregnation. This preliminary treatment optimizes the sheet properties for impregnation while maintaining sufficient structural integrity for handling through controlled processing parameters.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method improves fiber impregnation, reduces material creep, and achieves prepregs with enhanced mechanical properties, such as a flexural modulus greater than 20 GPa and breaking strength greater than 400 MPa, suitable for high-speed industrial production with reduced waste.

Implementation Method 1

heating the complex to a temperature higher than the melting temperature of the thermoplastic material so that the thermoplastic material impregnates the fibers

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 2

heating while applying pressure higher than atmospheric pressure on the complex

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS12138869B2Method for manufacturing a prepreg made of a composite material
Publication Date: 2024.11.12 INST DE RECH TECHQUE JULES VERNE
  • US12138869B2 patent drawing
  • US12138869B2 patent drawing
  • US12138869B2 patent drawing

AI summary

The method comprises the following consecutive steps: providing at least one reinforcement layer and at least one matrix sheet made of thermoplastic material; forming a complex with the reinforcement layer and the matrix sheet; and placing the complex in a production tool so that the thermoplastic material impregnates the fibers of the reinforcement layer(s) in order to form a prepreg. The method comprises, in the production tool, the following consecutive steps: heating the complex to a temperature higher than the melting temperature of the thermoplastic material without applying pressure; heating the complex to a temperature higher than the melting temperature of the thermoplastic material while applying a production pressure higher than atmospheric pressure.