Thermoresponsive Paste Coating for Li-Ion Battery Electrodes

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Solution Overview

Problem

The production of lithium-ion battery electrodes faces challenges such as binder migration during drying, leading to poor adhesion and electrochemical performance, especially with rapid drying methods, and issues with inhomogeneous surface weights and particle alignment due to low solids content and anisotropic particle shapes.

Innovation Solution

A thermoresponsive paste is developed by adding a solidifying additive, such as methyl cellulose, to conventional pastes, which suppresses binder migration and enhances particle alignment and homogeneity, allowing for faster and more efficient drying without compromising adhesion or particle orientation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If rapid drying is used to increase productivity, then drying speed is improved, but binder migration occurs leading to poor adhesion

Engineering Contradiction:
Improvedrying speedVSAvoidadhesion quality
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention changes the physical-chemical parameters of the paste by adding a solidifying agent, transforming it into a thermoresponsive paste that solidifies at elevated temperatures. This allows rapid drying without binder migration because the solidified matrix prevents particle movement even under strong convective conditions.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The solidifying agent is added to the paste before application, so that upon heating during drying, the paste pre-solidifies forming a stable matrix that locks particles in place. This preliminary structural change prevents the harmful binder migration that would otherwise occur during rapid drying.

Inventive Principle:
Principle #10Preliminary action

2Ease of operation

If low solids content paste is used to maintain flowability, then application is improved, but convection during drying causes particle migration and inhomogeneous surface weight

Engineering Contradiction:
Improveapplication flowabilityVSAvoidsurface weight homogeneity
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The paste's rheological parameters are changed by incorporating a solidifying agent that triggers gelation at processing temperatures. This creates a thermoresponsive system that remains flowable during application but solidifies during drying, preventing convection-driven particle migration while maintaining application ease.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention introduces dynamic rheological properties to the paste through the solidifying agent. The paste transitions from a flowable state during application to a solidified state during drying, allowing the system to adapt its properties to different process stages and eliminate surface weight inhomogeneity.

Inventive Principle:
Principle #15Dynamics

3Reliability

If vertical particle alignment is achieved to improve charging speed, then battery performance is improved, but drying convection disrupts alignment and causes crack formation

Engineering Contradiction:
Improvecharging speedVSAvoidparticle alignment stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The invention changes the thermal-rheological parameters of the paste by adding a solidifying agent that triggers rapid solidification at drying temperatures. This solidified matrix stabilizes the vertically aligned particles, preventing convection-induced disruption and crack formation while preserving the high-performance aligned structure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The solidifying agent provides beforehand cushioning by creating a rigidified matrix that protects the carefully aligned particle structure from convective disturbances during drying. This pre-established structural support prevents both alignment loss and crack formation.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

4Reliability

If mild drying conditions are used to prevent binder migration, then adhesion is improved, but manufacturing productivity decreases

Engineering Contradiction:
Improveadhesion qualityVSAvoidmanufacturing speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The invention fundamentally changes the paste's thermal response by adding a solidifying agent, enabling it to withstand rapid drying conditions. This allows the system to achieve both high productivity through fast drying and high reliability through prevented binder migration, eliminating the need for mild drying conditions.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of thermoresponsive pastes results in improved adhesion, homogeneous basis weights, and maintained particle alignment, accelerating the electrode manufacturing process while preventing defects like cracks and inhomogeneities, even with low solids content and anisotropic particles.

Implementation Method 1

a thermoresponsive paste which contains solid particles and a thermoresponsive component... the coating or layer is applied to a support, solidified and dried

Methodology Applied
Scientific EffectThermoresponsive solidification: Phase Change

Implementation Method 2

At least 0.001% and less than 80% of a volatile component is removed from the coating during solidification

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP3759176B1Method for producing a coating
Publication Date: 2022.07.13 BATTRION AG
  • EP3759176B1 patent drawingFigure 1
  • EP3759176B1 patent drawingFigure 2

AI summary

The invention relates to a method for producing a coating, which can be used in particular to produce electrodes, in particular to produce electrodes for use in lithium ion batteries. A method for producing a coating from a thermoresponsive paste, which contains solid particles and a thermoresponsive component, the coating or layer being applied to substrate, solidified and dried, characterized in that less than 80% of a volatile solvent component is removed from the coating during the solidification.