Ultra-Efficient Sulfur Curing System for Tire Tread

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Solution Overview

Problem

Tire designers face a compromise between tire wear and wet braking performance, as improving one characteristic often results in a decline in the other, particularly due to the trade-off between polybutadiene content in the tread's rubber composition.

Innovation Solution

A tire tread composition featuring a cross-linkable elastomer with high unsaturated diene elastomer and inorganic reinforcing filler, combined with a plasticizing system and an ultra-efficient sulfur curing system, which maintains good material cohesion and improves traction.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of stationary object

If polybutadiene content in the tread's rubber composition is increased to improve tire wear, then tire wear is improved, but wet braking performance deteriorates

Engineering Contradiction:
Improvetire wearVSAvoidwet braking performance
Core Design Contradiction:
Duration of action of stationary objectVSReliability

Solution Approach 1:

The patent applies parameter changes by optimizing the sulfur to accelerator weight ratio to between 0.02 and 0.2, which is a significant deviation from conventional ratios. This parameter adjustment enables the rubber composition to achieve both improved wear resistance and maintained wet braking performance by controlling the cross-linking density and network structure of the vulcanized rubber

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by combining highly unsaturated diene elastomer with specific inorganic reinforcing fillers (such as silica or carbon black) in optimized proportions. This composite approach allows the tread to simultaneously achieve enhanced wear resistance through filler reinforcement and good wet braking performance through the elastomer's inherent properties

Inventive Principle:
Principle #40Composite materials

2Reliability

If polybutadiene content is decreased to improve wet braking performance, then wet braking performance is improved, but tire wear deteriorates

Engineering Contradiction:
Improvewet braking performanceVSAvoidtire wear
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent changes the sulfur to accelerator ratio parameter to a low range (0.02-0.2) and adjusts the inorganic filler content to between 95-160 phr, creating a vulcanization system that achieves optimal balance between wet braking performance and wear resistance without relying on high polybutadiene content

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite materials consisting of diene elastomer blended with inorganic reinforcing fillers in specific proportions, where the filler provides wear resistance while the elastomer matrix maintains wet braking performance, eliminating the need to sacrifice one property for the other

Inventive Principle:
Principle #40Composite materials

3Force

If inorganic reinforcing filler content is increased to improve traction, then traction is improved, but material cohesion deteriorates

Engineering Contradiction:
ImprovetractionVSAvoidmaterial cohesion
Core Design Contradiction:
ForceVSStrength

Solution Approach 1:

The patent applies parameter changes by optimizing the sulfur to accelerator ratio to between 0.02 and 0.2, which controls the cross-linking density and ensures that even with high inorganic filler content (95-160 phr), the rubber matrix maintains sufficient material cohesion and prevents chunking

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses an intermediary ultra-efficient vulcanization system that acts as a mediator between the inorganic reinforcing fillers and the rubber matrix. This vulcanization system, with its optimized sulfur to accelerator ratio, creates effective bonding between filler particles and rubber, ensuring both high traction from filler reinforcement and good material cohesion from proper cross-linking

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides improved traction while maintaining material cohesion, reducing chunking and extending the tire's operational life, making it suitable for all-weather and summer tires.

Implementation Method 1

The rubber composition is cured with an ultra-efficient sulfur curing system having a sulfur to accelerator weight ratio adjusted between 0.02 and 0.2 to provide the rubber composition with an MA300/G* ratio of greater than 1.7

Methodology Applied
Scientific EffectVulcanization: Chemical Bonding

Implementation Method 2

The composition may further include between 60 phr and 130 phr of a plasticizing system comprising a plasticizing resin having a Tg of at least 25 °C and a plasticizing liquid. The rubber composition has a glass transition temperature of between -35 °C and 0 °C

Methodology Applied
Scientific EffectGlass transition: Phase Change

Data Source

PatentEP2748248B1Tread with ultra efficient vulcanization system
Publication Date: 2018.03.07 MICHELIN & CO (CIE GEN DES ESTAB MICHELIN)

AI summary

Tire treads having improved traction properties while surprisingly still maintaining good material cohesion properties, the tire treads comprising a rubber composition based upon a highly unsaturated diene elastomer and between 95 phr and 160 phr of an inorganic reinforcing filler. The composition may further include between 60 phr and 130 phr of a plasticizing system made up of a plasticizing resin having a Tg of at least 25 °C and a plasticizing liquid. The rubber composition is cured with an ultra-efficient sulfur curing system having a sulfur to accelerator weight ratio adjusted between 0.02 and 0.2 to provide the rubber composition with an MA300/G* ratio of greater than 1.7, wherein the elongation modulus MA300 at 300 % is measured at 23 °C and the shear modulus G* is measured at 60 °C.