Tissue Sample Preparation System Morphology Preservation

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Solution Overview

Problem

Existing tissue clearing methods using organic solvents cause significant shrinkage and morphological changes, leading to loss of biologically important 3D information, while water-based methods do not provide sufficient optical clarity.

Innovation Solution

A method involving fixation, delipidation with a chaotropic agent, dehydration, and organic clearing, which includes a chaotropic agent to induce swelling to counteract shrinkage, ensuring minimal deviation in volume and morphology, combined with selective photo bleaching to enhance clarity and reduce autofluorescence.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If organic solvent based clearing methods are used, then optical clarity is improved, but tissue shrinkage and morphological changes occur

Engineering Contradiction:
Improveoptical clarityVSAvoidtissue morphology
Core Design Contradiction:
Illumination intensityVSManufacturing precision

Solution Approach 1:

The clearing process is divided into multiple sequential steps: dehydration with organic solvent, clearing with high-refractive-index organic solvent, and post-clearing treatment with water-based solution. This segmentation allows each step to optimize for its specific function while minimizing overall tissue damage

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Dehydration with organic solvent is performed as a preliminary step before clearing to remove water and prepare the tissue for subsequent clearing steps, preventing water-solvent mixing issues and improving clearing efficiency

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If water based clearing methods are used, then tissue morphology is preserved, but optical clarity is insufficient

Engineering Contradiction:
Improvetissue morphologyVSAvoidoptical clarity
Core Design Contradiction:
Manufacturing precisionVSIllumination intensity

Solution Approach 1:

The refractive index of the clearing medium is changed from water-based (low RI) to organic solvent-based (high RI matching tissue), dramatically improving optical clarity while post-clearing treatments restore morphological fidelity

Inventive Principle:
Principle #35Parameter changes

3Illumination intensity

If organic solvents are used for clearing, then light scattering is reduced, but fluorescent protein emission is quenched

Engineering Contradiction:
Improvelight transmissionVSAvoidfluorescent signal
Core Design Contradiction:
Illumination intensityVSLoss of information

Solution Approach 1:

The harmful quenching effect of organic solvents on fluorescent proteins is converted into a beneficial timing strategy: clearing is performed first to optimize light transmission, then fluorescent staining is applied afterward when the tissue is already cleared but fluorescent proteins have not yet been exposed to quenching conditions

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Data Source

PatentEP3732461B1Tissue sample preparation system
Publication Date: 2026.01.21 F HOFFMANN LA ROCHE & CO AG
  • EP3732461B1 patent drawingFigure 1
  • EP3732461B1 patent drawingFigure 2
  • EP3732461B1 patent drawingFigure 3A~3B

AI summary

The invention relates to a method (100) of preparing a biological tissue sample (301) for optical analysis such that a deviation of the volume and/or morphology of the prepared sample from the volume or morphology of the original tissue is minimized. The method comprises: − a) fixing (102) the tissue sample with a first fixation solution (202); − b) immersing (104) the tissue sample in a delipidation solution (204) comprising a chaotropic agent adapted to induce a swelling of the sample; − d) staining (108) the tissue sample; − f) dehydrating (112) the tissue sample in an organic dehydration solution (210), the dehydration solution adapted to induce a shrinking of the sample; and − g) immersing (114) the fixed tissue sample in an organic clearing solution (212).