Titanium Aluminide Sintering via Reactive Powder

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

The high energy costs and tooling degradation associated with sintering titanium aluminide parts using conventional powder metallurgy techniques, which require temperatures close to the melting point, leading to inefficient energy use and increased maintenance costs.

Innovation Solution

A composition comprising a mixture of titanium aluminide powder and a mixture of metallic aluminum and titanium powders, which initiates sintering at lower temperatures through an exothermic chemical reaction, reducing energy needs and maintaining part density, while minimizing tooling degradation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If sintering is performed at very high temperatures (close to melting point, 1380-1450°C) to achieve complete sintering and high density, then density of the part is improved, but energy consumption increases and tooling lifetime decreases

Engineering Contradiction:
ImprovedensityVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The invention changes the chemical composition parameters of the powder mixture by adding reactive aluminum powder (5-20 wt%) to the titanium aluminide powder. This compositional change enables an exothermic reaction during sintering that provides internal heat, allowing complete sintering at lower temperatures (1200-1350°C) while achieving the same high density (≥95%) as conventional high-temperature sintering

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention converts the potentially harmful effect of high temperature requirements into a benefit by utilizing the exothermic reaction between aluminum and titanium. The reaction heat that would normally be a byproduct is harnessed to provide the necessary sintering energy, eliminating the need for external high-temperature heating and reducing overall energy consumption while maintaining high density

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Use of energy by moving object

If sintering temperature is reduced to save energy, then energy consumption decreases, but density of the sintered part becomes insufficient

Engineering Contradiction:
Improveenergy consumptionVSAvoiddensity
Core Design Contradiction:
Use of energy by moving objectVSManufacturing precision

Solution Approach 1:

The invention makes the sintering process self-service by incorporating reactive aluminum powder that generates its own heat through exothermic reaction with titanium during sintering. This internal heat generation eliminates dependence on external high-temperature heating, enabling the process to achieve complete sintering and high density at lower overall temperature levels with reduced energy input

Inventive Principle:
Principle #25Self-service

3Manufacturing precision

If sintering is performed at high temperatures to achieve complete densification, then density is improved, but tooling degradation increases and maintenance costs rise

Engineering Contradiction:
ImprovedensityVSAvoidtooling lifetime
Core Design Contradiction:
Manufacturing precisionVSDuration of action of stationary object

Solution Approach 1:

The invention changes the temperature parameter of the sintering process from 1380-1450°C to 1200-1350°C by introducing reactive aluminum powder. This temperature reduction protects the tooling from excessive thermal stress and degradation, extending tooling lifetime and reducing maintenance costs while still achieving complete densification (≥95% density) through the exothermic reaction

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution allows for reduced energy consumption and uniform sintering, achieving higher part density with lower sintering temperatures, thus reducing production costs and extending tooling lifespan.

Implementation Method 1

a chemical reaction is initiated between the metallic aluminum and the metallic titanium for forming a titanium aluminide. This chemical reaction is exothermic and delivers energy in the form of heat to the composition

Methodology Applied
Scientific EffectExothermic reaction: Exothermic Reaction

Implementation Method 2

When the temperature of the composition is close to the melting temperature of metallic aluminum (about 660° C.), the grains of metallic aluminum begin to melt

Methodology Applied
Scientific EffectMelting: Melting

Data Source

PatentUS10995389B2Composition for fabricating parts out of titanium aluminide by sintering powder, and a fabrication method using such a composition
Publication Date: 2021.05.04 SAFRAN AIRCRAFT ENGINES SAS
  • US10995389B2 patent drawing

AI summary

A composition for sintering to fabricate a part comprising an alloy based on titanium aluminide, the composition including a powder of an alloy based on titanium aluminide, and an addition powder including a mixture of a metallic aluminum powder and of a metallic titanium powder. The composition includes 0.5% to 5% by weight of addition powder.