Titanium Carbide Nanoparticle Electric Resistance Control

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Solution Overview

Problem

Current methods for producing titanium carbide nanoparticles do not effectively control physical properties other than particle size, limiting their application and functionality.

Innovation Solution

The method involves varying the oxygen concentration of titanium carbide nanoparticles by adjusting the amount of carbon source in the production process using a thermal plasma flame, allowing for the control of desired electric resistance properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional production methods (baking oxidized titanium and carbon in non-oxidizing atmosphere or hydrogen atmosphere) are used, then titanium carbide nanoparticles can be produced, but the physical properties other than particle size cannot be controlled

Engineering Contradiction:
Improvecontrol of physical propertiesVSAvoidapplication expansion
Core Design Contradiction:
Manufacturing precisionVSAdaptability or versatility

Solution Approach 1:

The patent applies parameter changes by controlling the oxygen concentration in the reaction atmosphere during thermal plasma processing to precisely control the physical properties (such as electric resistance) of titanium carbide nanoparticles. By adjusting the oxygen concentration parameter, the invention enables production of nanoparticles with desired electrical characteristics while maintaining nanoparticle formation, thus resolving the contradiction between manufacturing precision and adaptability.

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If particle size control methods (adding Co or Ni, controlling primary particle size) are used, then homogeneous titanium carbide powder can be obtained, but other physical properties remain uncontrollable

Engineering Contradiction:
Improveparticle size controlVSAvoidfunctionality
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The invention introduces a new control parameter (oxygen concentration) that independently affects physical properties without interfering with particle size control. This allows simultaneous achievement of homogeneous particle size distribution and desired physical properties, resolving the contradiction between manufacturing precision and reliability.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If thermal plasma flame method is used with varied carbon source amount, then oxygen concentration and electric resistance can be controlled, but process complexity increases

Engineering Contradiction:
Improveelectric resistance controlVSAvoidproduction process
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent utilizes the thermal plasma flame method and varies the carbon source amount to control oxygen concentration and electric resistance. This approach achieves precise control of physical properties through parameter adjustment in an existing production framework, balancing manufacturing precision with acceptable process complexity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the production of titanium carbide nanoparticles with specific electric resistance values, enhancing their functionality and expanding their applications.

Implementation Method 1

a production step for producing titanium carbide nanoparticles using titanium powder or titanium oxide powder, a carbon source and a thermal plasma flame

Methodology Applied
Scientific EffectThermal plasma: Plasma

Implementation Method 2

perform reduction and carbonization in a hydrogen atmosphere at a temperature of 1,500 to 1,750° C.

Methodology Applied
Scientific EffectThermal energy: Heating

Implementation Method 3

the volume resistance (electric resistance) of titanium carbide nanoparticles varies in value with the oxygen concentration thereof

Methodology Applied
Scientific EffectOxygen concentration control:

Data Source

PatentUS9751769B2Method for production of titanium carbide nanoparticles
Publication Date: 2017.09.05 NISSHIN ENG
  • US9751769B2 patent drawing
  • US9751769B2 patent drawing
  • US9751769B2 patent drawing

AI summary

A method for production of titanium carbide nanoparticles, the method having: a step for supplying titanium powder or titanium oxide powder into a thermal plasma flame; and a step for producing titanium carbide nanoparticles by supplying a reactive gas as a cooling gas and as a source of carbon at the downstream end of the thermal plasma flame. By varying the supplied quantity of the reactive gas, the oxygen concentration of the produced titanium carbide nanoparticles is varied. Therefore, for example, titanium carbide nanoparticles having different volume resistivity values can be produced.