Titanium Oxide Anode Composition for Fast-Charging Li-Ion Batteries

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Solution Overview

Problem

Lithium ion secondary batteries face limitations in capacity and electron conductivity, particularly with titanium oxide-based negative electrodes, which hinder high input and output characteristics.

Innovation Solution

Incorporating titanium oxide particles represented by the formula H2Ti12O25 with 0.3-5.0 weight percent single wall carbon nanotubes into the negative electrode to enhance electron conductivity and improve input and output characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If Li4Ti5O12 is used as negative electrode material to avoid lithium deposition, then discharge and charge potential is improved (1.5V vs Li/Li+), but electron conductivity is low requiring conductive agents which decrease capacity

Engineering Contradiction:
Improvelithium deposition preventionVSAvoidbattery capacity
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent uses a composite structure where Li4Ti5O12 particles are combined with conductive carbon materials (graphite, carbon black, or conductive polymer) to create a negative electrode that maintains both high discharge potential (avoiding lithium deposition) and sufficient electron conductivity. The conductive agent forms a network around the Li4Ti5O12 particles, ensuring electron transport while the low amount used (1-20 wt%) minimizes capacity loss.

Inventive Principle:
Principle #40Composite materials

2Productivity

If high input charging is implemented to achieve short charging time, then charging speed is improved, but high overvoltage causes lithium deposition on graphite negative electrodes

Engineering Contradiction:
Improvecharging speedVSAvoidlithium deposition
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent changes the electrochemical potential parameter of the negative electrode by using Li4Ti5O12 with a discharge potential of 1.5V vs Li/Li+, which is significantly higher than graphite's potential. This parameter change allows the battery to accept high input charging currents without causing lithium deposition, as the higher potential prevents the thermodynamic conditions for lithium plating on the negative electrode.

Inventive Principle:
Principle #35Parameter changes

3Power

If conductive agents are added to improve electron conductivity of Li4Ti5O12, then electron conductivity is improved, but capacity is extremely decreased

Engineering Contradiction:
Improveelectron conductivityVSAvoidcapacity
Core Design Contradiction:
PowerVSQuantity of substance

Solution Approach 1:

The patent applies local quality by concentrating the conductive agent specifically at the particle surfaces and inter-particle regions of Li4Ti5O12, rather than uniformly mixing throughout the electrode. The conductive carbon materials form localized conductive networks and coatings on the Li4Ti5O12 particle surfaces, providing electron conductivity pathways exactly where needed for electron transport to and from the active material, while minimizing the overall amount of conductive agent required.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The combination of H2Ti12O25 with single wall carbon nanotubes improves electron conductivity, leading to enhanced input and output characteristics and increased capacity without compromising mechanical strength.

Implementation Method 1

The negative electrode contains titanium oxide particles that are particles of titanium oxide represented by general formula H2Ti12O25, a binder, and 0.3-5.0 weight percent of single wall carbon nanotubes with respect to the titanium oxide

Methodology Applied
Scientific EffectElectrical conduction: Conduction (electrical)

Data Source

PatentUS20240258560A1Nonaqueous electrolyte secondary battery
Publication Date: 2024.08.01 NISSHA PRINTING CO LTD

AI summary

Disclosed is a nonaqueous electrolyte secondary battery having improved electron conductivity of an electrode and improved input and output characteristics. The nonaqueous electrolyte secondary battery includes a positive electrode containing a lithium-containing transition metal composite oxide as an active material, a negative electrode, and a nonaqueous electrolyte. The negative electrode contains titanium oxide particles that are particles of titanium oxide represented by general formula H2Ti12O25, a binder, and 0.3-5.0 weight percent of single wall carbon nanotubes with respect to the titanium oxide. The titanium oxide particles have a secondary particle size D50 of 1 to 15 μm and a secondary particle size D90 of 50 μm or less.