Titanium Surface Functionalization with Nanometric TiO2 Particles

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Solution Overview

Problem

Titanium metal surfaces used in implantology, particularly in orthodontic parts, lack effective bactericidal and bacteriostatic properties, posing a challenge for preventing infections.

Innovation Solution

A process involving immersion of titanium articles in a suspension of nanometric titanium dioxide particles, followed by solvent removal and a thermal cycle to fix the nanoparticles onto the surface, enhancing bactericidal or bacteriostatic properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If titanium metal surfaces are used in implantology, then biocompatibility and durability are improved, but bactericidal and bacteriostatic properties are insufficient

Engineering Contradiction:
Improvebactericidal and bacteriostatic propertiesVSAvoidbacterial infection risk
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent applies composite materials by combining titanium metal substrate with nanometric titanium dioxide particles. The nanoparticles are deposited onto the titanium surface and fixed through thermal treatment, creating a composite structure that retains the biocompatibility of titanium while adding bactericidal properties through the photocatalytic activity of TiO2 nanoparticles.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent applies local quality by modifying only the surface properties of the titanium implant rather than the bulk material. The nanometric TiO2 particles are deposited and fixed specifically on the surface, creating a localized functional layer that provides bactericidal activity while maintaining the overall structural integrity and biocompatibility of the titanium implant.

Inventive Principle:
Principle #3Local quality

2Reliability

If nanometric titanium dioxide particles are deposited on titanium surface, then bactericidal properties are improved, but manufacturing complexity increases

Engineering Contradiction:
Improvebactericidal actionVSAvoidsurface treatment process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by utilizing thermal treatment parameters (temperature and time) to control the fixation of nanoparticles onto the titanium surface. By adjusting these parameters, the process achieves effective bonding of TiO2 nanoparticles while maintaining a relatively simple manufacturing procedure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces complex mechanical or chemical bonding methods with a thermal treatment process. The thermal cycle facilitates the fixation of nanoparticles through controlled heating, simplifying the overall manufacturing process compared to alternative methods such as mechanical attachment or complex chemical bonding agents.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Strength

If thermal cycle is applied to fix nanoparticles, then bonding strength is improved, but energy consumption increases

Engineering Contradiction:
Improvenanoparticle fixation strengthVSAvoidthermal treatment energy
Core Design Contradiction:
StrengthVSUse of energy by moving object

Solution Approach 1:

The patent optimizes the thermal treatment parameters (temperature range, treatment time, and heating rate) to achieve effective nanoparticle fixation while minimizing energy consumption. By carefully controlling these parameters, the process achieves strong bonding without requiring excessive thermal energy.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The treated titanium surfaces exhibit significant bactericidal or bacteriostatic action, effectively reducing the risk of infections in orthodontic and other prosthetic parts.

Implementation Method 1

when completely wetted the article is heated to remove the solvent

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

the article is subjected to a thermal cycle in order to improve fixing of the nanoparticles to the treated surface

Methodology Applied
Scientific EffectThermal treatment: Heat Treatment

Data Source

PatentUS8118923B2Process for functionalizing titanium metal surfaces with nanometric particles of titanium and products thus functionalized
Publication Date: 2012.02.21 COLOROBBIA ITALA

AI summary

A method is described which enables antibacterial properties to be attributed to a titanium surface by applying titanium dioxide suspensions of nanometric dimensions.