TM-NQR Detection via RF Temperature Modulation

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Solution Overview

Problem

Conventional Nuclear Quadrupole Resonance (NQR) techniques face challenges due to temperature dependence, weak signal strength, and susceptibility to noise interference, making them inefficient for substance detection in certain applications, especially in cluttered or dynamic environments.

Innovation Solution

A system utilizing a pulsed high-frequency field source and a radio frequency heater to induce temperature changes in a target, generating multiple NQR spectral datasets, which are then analyzed to classify the presence of substances of interest using a classifier, thereby exploiting temperature-dependent spectral shifts to enhance detection accuracy and reduce noise interference.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional NQR techniques are used for substance detection, then detection capability is provided, but temperature measurement requirements increase device complexity and measurement time

Engineering Contradiction:
Improvedetection capabilityVSAvoidtemperature measurement equipment
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by deliberately varying the temperature of the target material through RF heating and observing the resulting changes in NQR signal characteristics. Instead of measuring temperature as a separate parameter to correct for its effects, the system uses temperature-induced spectral shifts as the detection mechanism itself, thereby eliminating the need for separate temperature measurement equipment while maintaining detection reliability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the harmful effect of temperature dependence into a beneficial detection mechanism. The temperature sensitivity that previously required correction is now exploited as the primary detection signal. By applying RF heating and observing the resulting spectral changes, the system transforms temperature variability from a nuisance factor into a useful detection parameter, eliminating the need for separate temperature measurement equipment.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Measurement precision

If temperature measurement is performed in conventional NQR, then detection accuracy is maintained, but substance sensing time and throughput are reduced

Engineering Contradiction:
Improvedetection accuracyVSAvoidsubstance sensing throughput
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent merges the temperature measurement function with the NQR detection function into a single simultaneous process. By applying RF heating and acquiring NQR spectra at different temperatures concurrently, the system eliminates the sequential steps of separate temperature measurement and NQR detection, thereby maintaining detection accuracy while significantly improving sensing throughput.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent implements continuous useful action by maintaining RF heating during the NQR spectral acquisition process. Instead of performing temperature measurement as a discrete preliminary step followed by detection, the system continuously applies heating and continuously acquires spectra, allowing temperature-induced spectral changes to be observed in real-time without interrupting the detection process, thus improving throughput.

Inventive Principle:
Principle #20Continuity of useful action

3Reliability

If NQR signals are measured in cluttered environments, then detection is attempted, but signal strength and noise resistance are insufficient

Engineering Contradiction:
Improvedetection capabilityVSAvoidnoise interference
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent applies dynamics by introducing time-varying temperature conditions through RF heating during the measurement process. The NQR spectral characteristics change dynamically with temperature, creating a time-dependent signal pattern that can be distinguished from static noise. This dynamic modulation of the signal through temperature changes enhances the signal-to-noise ratio in cluttered environments by making the signal distinguishable from background noise.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements feedback by monitoring the NQR spectral changes in response to RF heating and using this information to identify the presence of target materials. The system continuously acquires spectra during heating and compares the temporal evolution of spectral features against reference patterns, allowing real-time feedback that enhances detection reliability in noisy environments by filtering out static interference.

Inventive Principle:
Principle #23Feedback

4Measurement precision

If multiple NQR spectral datasets are collected at different temperatures, then detection accuracy improves, but measurement time increases

Engineering Contradiction:
Improvedetection accuracyVSAvoidmeasurement time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent applies periodic action by using pulsed RF heating cycles that alternately heat and cool the target material while acquiring NQR spectra at regular intervals. This periodic heating-cooling cycle enables the collection of multiple temperature-dependent spectral datasets in a systematic sequence, capturing the temporal evolution of spectral features without requiring continuous heating, thereby reducing total measurement time while maintaining detection accuracy.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach improves detection accuracy, reduces false alarms and misses, and provides a practical, fieldable solution to the limitations of conventional NQR techniques by leveraging temperature-dependent spectral changes and minimizing noise interference.

Implementation Method 1

a pulsed high frequency (HF) field source, configured to establish in a detection space a pulsed HF excitation field configured to excite NQR resonance of a component material of a target of interest

Methodology Applied
Scientific EffectNuclear Quadrupole Resonance: Resonance

Implementation Method 2

a radio frequency (RF) heater, configured to illuminate a TI while in the pulsed HF excitation field in the detection space, with an RF energy configured to effect a temperature increase in the TI

Methodology Applied
Scientific EffectDielectric Heating: Dielectric Heating

Data Source

PatentUS12038489B2System for radio frequency illumination based temperature modulated-nuclear quadrupole resonance (TM-NQR) and signature detection of potential threat materials
Publication Date: 2024.07.16 THE TRUSTEES OF PRINCETON UNIV
  • US12038489B2 patent drawing
  • US12038489B2 patent drawing
  • US12038489B2 patent drawing

AI summary

Systems and methods are described, and one method includes illuminating a target-of-interest (TI) with an RF energy configured to effect, over a time duration extending from a first time to a second time, an increase in a temperature of the TI. At a first detection time within the time duration, a first temperature NQR signal spectrum of the TI is detected, and a corresponding first temperature NQR spectrum data set is generates. At a second detection time, subsequent to the first detection time, a second temperature NQR signal spectrum of the TI is detected and corresponding second temperature NQR spectrum data set is output. Based at least in part on the first temperature NQR spectral dataset and the second temperature NQR spectral dataset, the TI is classified between including the SI and not including the SI.