Toner Composition with Composite Polyester Resins for Fixability

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Solution Overview

Problem

Current toners for high-speed printing lack sufficient low-temperature fixability and hot offset resistance, leading to image density fluctuations and fogging issues, especially after long-term printing.

Innovation Solution

A toner composition featuring a blend of polyester resins with different softening points, where one resin has a high softening point and the other a low softening point, both derived from aromatic diols, with specific polyhydric alcohol and polyvalent carboxylic acid units, ensuring uniform dispersion and improved stability through oxyalkylene ether and aliphatic dicarboxylic acid components.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If the glass transition point and softening point of the binder resin are reduced to achieve low-temperature fixability, then the fixability at low temperature is improved, but the hot offset resistance is reduced

Engineering Contradiction:
Improvefixation temperatureVSAvoidhot offset resistance
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The invention uses a composite binder resin system consisting of a polyester resin base and a polyether-modified polyester resin. The polyester resin provides hot offset resistance through its higher softening point, while the polyether-modified component contributes to low-temperature fixability by reducing the glass transition point. This composite structure allows simultaneous achievement of both low-temperature fixability and hot offset resistance that cannot be obtained with a single resin type.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention modifies the molecular structure parameters of the polyester resin by introducing polyether chains through modification. This changes the glass transition point and softening point parameters of the resin, enabling the material to exhibit both low-temperature flexibility and high-temperature stability. The specific parameter adjustment involves controlling the polyether content and molecular weight to optimize the balance between fixability and hot offset resistance.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If polyester resins with different softening points are used to achieve compatibility between low-temperature fixability and hot offset resistance, then both properties are improved to some level, but the fixability is insufficient for high-speed printing requiring about 100 sheets per minute

Engineering Contradiction:
Improvehot offset resistanceVSAvoidprinting speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The invention optimizes the molecular weight and softening point parameters of the polyester resin to achieve rapid melting characteristics. By adjusting these parameters, the resin melts quickly at the fixing temperature, enabling high-speed printing. The specific parameter range is controlled to ensure both fast melting for high productivity and sufficient hot offset resistance.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If conventional toners are used for high-speed printing, then printing speed is maintained, but density fluctuation enlarges and fogging occurs in white portions after long-term printing

Engineering Contradiction:
Improveprinting speedVSAvoidimage density stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The invention employs a composite resin system that maintains toner particle integrity and uniformity during long-term high-speed printing. The combination of polyester resin and polyether-modified polyester resin prevents toner degradation, density fluctuation, and fogging by providing stable melting and solidification characteristics that preserve image quality over extended printing periods.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The toner achieves enhanced low-temperature fixability and hot offset resistance, reducing image density fluctuations and fogging, even after prolonged printing, by maintaining the durability and stability of the toner particles.

Implementation Method 1

The glass transition point and softening point of the binder resin of the toner are reduced, and a binder resin having sharp-melt property is used

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 2

The glass transition point and softening point of the binder resin of the toner are reduced

Methodology Applied
Scientific EffectGlass transition:

Implementation Method 3

the hot offset resistance of a toner that achieves low-temperature fixability is apt to reduce

Methodology Applied
Scientific EffectThermal stability:

Data Source

PatentEP2889691B1Toner and two-component developer
Publication Date: 2017.03.01 CANON KK
  • EP2889691B1 patent drawingFigure 1

AI summary

Provided is a toner obtained by melting and kneading a binder resin containing a polyester resin A and a polyester resin B, a colorant, and a wax, in which in the resin A, the content of a polyhydric alcohol unit derived from an aromatic diol, the content of a polyhydric alcohol unit derived from an oxyalkylene ether of a novolac type phenol resin, and the content of a polyvalent carboxylic acid unit derived from an aliphatic dicarboxylic acid, which contains a straight-chain hydrocarbon having 4 or more to 16 or less carbon atoms as a main chain and has carboxyl groups at both of its terminals, fall within specific ranges, and in the resin B, the content of a polyhydric alcohol unit derived from an aromatic diol and the content of a polyvalent carboxylic acid unit derived from an aromatic dicarboxylic acid or a derivative thereof fall within specific ranges.