Tooling Fixture Coatings for Clean CMC Preform Release

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Solution Overview

Problem

Delamination of ceramic matrix composite (CMC) preforms occurs during detooling from tooling fixtures, leading to damage and the need for restarting the process with new preforms.

Innovation Solution

Application of coatings such as ceramic materials, hexagonal boron nitride, turbostratic boron nitride, and graphite on tooling fixture surfaces to facilitate preform release without delamination, while also sealing the fixture to prevent residue contamination during chemical vapor infiltration (CVI) processing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Shape

If perforated tooling is used to hold preforms during densification, then the preform maintains proper shape and geometry, but delamination occurs during detooling

Engineering Contradiction:
Improvepreform shape and geometryVSAvoidpreform integrity during detooling
Core Design Contradiction:
ShapeVSReliability

Solution Approach 1:

A coating layer is applied to the tooling fixture surfaces as an intermediary between the tooling and preform. This coating prevents direct adhesion while maintaining the structural support function of the tooling, thereby preventing delamination during detooling while preserving preform shape and geometry throughout the densification process

Inventive Principle:
Principle #24Intermediary (Mediator)

2Strength

If tooling fixture is used to maintain preform rigidity, then proper shape is maintained, but preform sticks to tooling causing damage

Engineering Contradiction:
Improvepreform rigidityVSAvoidadhesion between preform and tooling
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The coating serves as a mediator that eliminates harmful adhesion while preserving the beneficial mechanical support. The coating layer is applied to all tooling fixture surfaces including hole surfaces, creating a non-sticking interface that prevents preform damage during removal while maintaining preform rigidity during the densification process

Inventive Principle:
Principle #24Intermediary (Mediator)

3Ease of manufacture

If tooling fixture surfaces are exposed during CVI process, then manufacturing is simplified, but residue contamination occurs

Engineering Contradiction:
Improvetooling fixture manufacturingVSAvoidresidue contamination of preform
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The coating acts as a protective intermediary layer on all tooling fixture surfaces including the interior hole surfaces. This coating prevents direct contact between the preform and tooling residue, thereby preventing contamination while maintaining manufacturing simplicity. The coating is applied to all surfaces that would otherwise be exposed to the preform during the CVI process

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Prevents preform delamination and residue contamination, ensuring successful completion of the CVI process without the need for new preforms.

Implementation Method 1

The coating is disposed on the first surface and surfaces defining the plurality of holes. The coating comprises at least one of a ceramic material, hexagonal boron nitride, turbostratic boron nitride, and graphite.

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

at least partially densifying the fiber preform with a ceramic matrix through a process of chemical vapor infiltration

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Data Source

PatentEP4414346B1Coatings for tooling
Publication Date: 2025.12.03 RTX CORP
  • EP4414346B1 patent drawingFigure 1
  • EP4414346B1 patent drawingFigure 2~5
  • EP4414346B1 patent drawingFigure 6~8

AI summary

A tooling fixture (10) is disclosed for densification by chemical vapor infiltration of a fiber preform of a ceramic matrix composite. The tooling fixture (10) includes a body having oppositely disposed first and second surfaces (12, 14) and a plurality of holes (16) extending between the first and second surfaces (12, 14), and a coating (18). The first surface (12) is configured to be disposed adjacent to the fiber preform. The coating (18) is disposed on the first surface (12) and surfaces defining the plurality of holes (16). The coating (18) comprises at least one of a ceramic material, hexagonal boron nitride, turbostratic boron nitride, and graphite.