TPV Solid Polymer Electrolytes for Dendrite-Resistant Li-Ion Cells

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Solution Overview

Problem

Existing solid-state batteries face issues with lithium dendrite growth, limited lifetime, and safety concerns due to flammable liquid electrolytes, while existing polymer electrolytes lack sufficient ionic conductivity and mechanical strength, and are not easily reprocessable.

Innovation Solution

Development of thermoplastic vulcanizate (TPV) based solid polymer electrolytes (SPEs) comprising a crosslinked elastomer phase and a thermoplastic polymer phase, with specific ratios and additives to enhance mechanical properties and ionic conductivity, allowing for a cost-effective and efficient industrial production process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If liquid electrolytes are used in Li-ion batteries, then good mobility of Li+ cations is achieved, but flammability and thermal runaway risks increase

Engineering Contradiction:
Improvemobility of Li+ cationsVSAvoidflammability and thermal runaway
Core Design Contradiction:
SpeedVSObject-affected harmful factors

Solution Approach 1:

The patent changes the physical state parameter of the electrolyte from liquid to solid gel form, maintaining ionic conductivity while eliminating flammability risks associated with liquid electrolytes

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite gel electrolyte system combining crosslinked elastomer phase, thermoplastic polymer phase, and lithium salt, integrating the benefits of mechanical strength from polymers and ionic conductivity from lithium salts while eliminating liquid electrolyte hazards

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If polymer electrolytes are used to replace liquid electrolytes, then safety is improved, but ionic conductivity and mechanical strength are insufficient

Engineering Contradiction:
ImprovesafetyVSAvoidionic conductivity and mechanical strength
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent develops a composite gel electrolyte comprising crosslinked elastomer phase providing mechanical strength and flexibility, thermoplastic polymer phase providing structural integrity, and lithium salt providing ionic conductivity, achieving simultaneous improvement in all three properties

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent creates distinct phases with specialized functions: crosslinked elastomer domains provide mechanical strength and dendrite resistance, while thermoplastic polymer regions provide ionic transport pathways, optimizing local properties for specific functions

Inventive Principle:
Principle #3Local quality

3Strength

If completely crosslinked polymer electrolyte systems are used, then mechanical strength is improved, but reprocessability is lost

Engineering Contradiction:
Improvemechanical strengthVSAvoidreprocessability
Core Design Contradiction:
StrengthVSEase of manufacture

Solution Approach 1:

The patent segments the polymer system into two distinct phases: crosslinked elastomer phase providing mechanical strength and thermoplastic polymer phase maintaining reprocessability, allowing the material to exhibit both desired properties simultaneously

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent controls the degree of crosslinking to create a partial crosslinking state where sufficient crosslinks provide mechanical strength but enough uncrosslinked thermoplastic polymer remains to allow reprocessing and reshaping

Inventive Principle:
Principle #35Parameter changes

4Strength

If crystalline or vitreous polymers are used for mechanical reinforcement, then mechanical strength is improved, but ionic conductivity decreases

Engineering Contradiction:
Improvemechanical strengthVSAvoidionic conductivity
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent combines crystalline/vitreous polymer phases for mechanical reinforcement with amorphous gel phases containing lithium salts for ionic conductivity, creating a composite structure where each phase performs its optimal function

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent creates local amorphous regions within the polymer matrix where lithium ions can move freely, while maintaining overall crystalline or vitreous structure for mechanical strength, optimizing both properties through spatial differentiation

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The TPV SPEs exhibit improved electrochemical stability, high mechanical strength, resistance to lithium dendrite growth, and enhanced cyclability, making them suitable for high-performance solid-state batteries.

Implementation Method 1

a crosslinked elastomer phase and a thermoplastic polymer phase

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 2

ionic conductive solid electrolytes for solid state batteries notably to promote the safety of the systems

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Implementation Method 3

resistance to lithium dendrite growth, and enhanced cyclability

Methodology Applied
Scientific EffectMechanical resistance: Mechanical Force

Data Source

PatentEP4430692B1Thermoplastic vulcanizate compositions as solid polymer electrolytes
Publication Date: 2025.10.08 TOTALENERGIES ONETECH
  • EP4430692B1 patent drawingFigure 1~2
  • EP4430692B1 patent drawingFigure 3~4
  • EP4430692B1 patent drawingFigure 5~6

AI summary

The present application concerns solid polymer electrolytes (SPEs) comprising thermoplastic vulcanizates (TPVs) and alkali metal salts, their process of preparation and the electrochemical cells comprising such electrolytes.