Triblock Copolymer Gene Delivery via Segmented Self-Assembly

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Solution Overview

Problem

Current delivery systems for nucleic acids, such as siRNA, face challenges in efficiently targeting and internalizing into cells due to issues like toxicity, aggregation, and endosomal escape, limiting their therapeutic potential for applications like gene silencing and tissue regeneration.

Innovation Solution

Development of triblock copolymers with a hydrophilic, hydrophobic, and positively charged block structure that self-assemble into supramolecular structures like micelles or vesicles, allowing for reversible complexation with nucleic acids and enhanced cellular uptake, utilizing PEG, PPS, and peptides like TAT for efficient delivery.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If cationic polymers are used for gene delivery, then nucleic acid complexation is achieved, but toxicity and aggregation occur

Engineering Contradiction:
Improvenucleic acid delivery efficiencyVSAvoidtoxicity
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The cationic polymer is segmented into three distinct blocks: a hydrophilic block (PEG or PO) for solubility and biocompatibility, a hydrophobic block (PPS) for structural stability, and a cationic block (peptide or polyamine) for nucleic acid binding. This segmentation allows each block to perform its specific function while minimizing harmful effects.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the polymer have different properties: the hydrophilic block provides water solubility and reduces toxicity, the hydrophobic block provides structural stability, and the cationic block provides nucleic acid binding capability. This local differentiation of properties resolves the contradiction between delivery efficiency and toxicity.

Inventive Principle:
Principle #3Local quality

2Reliability

If cationic polymers self-assemble with nucleic acids, then complexation is formed, but aggregation occurs

Engineering Contradiction:
Improvenucleic acid complexationVSAvoidaggregation
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The polymer is divided into functional segments where the hydrophilic block maintains solubility and prevents aggregation, the hydrophobic block provides structural integrity, and the cationic block handles nucleic acid binding. This segmentation prevents the formation of large aggregates while maintaining effective complexation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The polymer's molecular weight, block ratios, and composition are optimized to control the self-assembly process. By adjusting these parameters, the system forms stable complexes without excessive aggregation, achieving both effective nucleic acid binding and compositional stability.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If viral vectors are used for gene delivery, then efficient internalization is achieved, but safety and immunogenicity issues arise

Engineering Contradiction:
Improveinternalization efficiencyVSAvoidimmunogenicity
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent uses synthetic polymers instead of complex viral vectors. These polymer-based delivery systems are simpler, non-immunogenic, and can be easily modified, avoiding the safety and immunogenicity issues associated with viral vectors while maintaining efficient internalization through endocytosis.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The cationic polymer acts as an intermediary carrier that facilitates nucleic acid internalization without requiring viral components. The polymer complexes with nucleic acids and mediates their uptake into cells through endocytosis, achieving efficient delivery without the immunogenicity of viral vectors.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Productivity

If endosomal escape is enhanced, then cytoplasmic delivery is improved, but cellular toxicity increases

Engineering Contradiction:
Improvecytoplasmic delivery efficiencyVSAvoidcellular toxicity
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The polymer's structure and function are made dynamic: the hydrophilic block provides water solubility and reduces toxicity, the hydrophobic block provides structural stability, and the cationic block provides nucleic acid binding. This dynamic design allows the system to navigate the endosomal pathway and achieve cytoplasmic delivery while minimizing cellular toxicity through the hydrophilic block's protective effects.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The triblock copolymer system enables effective internalization and release of nucleic acids within cells, overcoming previous delivery limitations and achieving significant gene silencing and therapeutic effects, such as downregulating target genes for conditions like postsurgical adhesions.

Implementation Method 1

a positively charged block capable of reversibly complexing a negatively charged molecule, e.g., a nucleic acid

Methodology Applied
Scientific EffectElectrostatic interaction: Electrostatics

Implementation Method 2

Polymers with novel triblock structures, containing spatially separated hydrophobic and hydrophilic parts, have been developed for the effective delivery of negatively charged molecules

Methodology Applied
Scientific EffectSelf-assembly: Self-Assembly

Implementation Method 3

a hydrophobic block disposed between the hydrophilic block and the positively charged block

Methodology Applied
Scientific EffectHydrophobic interaction: Hydrophobe

Data Source

PatentEP2298829B1Triblock copolymers for cytoplasmic delivery of gene-based drugs
Publication Date: 2017.09.20 ECOLE POLYTECHNIQUE FEDERALE DE LAUSANNE (EPFL)
  • EP2298829B1 patent drawingFigure 1
  • EP2298829B1 patent drawingFigure 2
  • EP2298829B1 patent drawingFigure 3A~3E

AI summary

The invention features a triblock copolymer including a hydrophilic block; a hydrophobic block; and a positively charged block capable of reversibly complexing a negatively charged molecule, e.g., a nucleic acid, wherein the hydrophobic block is disposed between the hydrophilic block and the positively charged block. Desirably, the triblock copolymer is capable of self-assembling into a supramolecular structure, such as a micelle or vesicle. The invention further features methods of delivering negatively charged molecules and methods of treating a disease or condition using the polymers of the invention.